1. Conditions are described for the separation and estimation of the neutral monosaccharides obtained on acidic hydrolysis of human gastric mucopolysaccharides. 2. The technique involves the formation of the trimethylsilyl derivatives of the sugars and the analysis of these by gas-liquid chromatography. 3. The monosaccharides estimated in gastric mucopolysaccharides by this technique were l-fuc...

The comparison of growth processes and fluorescent properties of CdZnTe semiconductor quantum dots that are synthesized in different concentrations of Zn2+ in water are discussed in this paper. The samples are characterized through absorbtion (UV) and photoluminescence spectra (PL). The results show that when the reaction time is prolonged, the absorption peak and fluorescent emission peak pres...

The comparison of growth processes and fluorescent properties of CdZnTe semiconductor quantum dots that are synthesized in different concentrations of Zn2+ in water are discussed in this paper. The samples are characterized through absorbtion (UV) and photoluminescence spectra (PL). The results show that when the reaction time is prolonged, the absorption peak and fluorescent emission peak pres...

In the present work, Bi2S3 nanostructures have been synthesized with the aid of thioglycollic acid (TGA) a solvent, capping agent, and sulfide source in the presence of ultrasonic method. The as-synthesized products were characterized by X-ray diffraction (XRD), Energy Dispersive X-ray spectroscopy (EDS), scanning electron microscope (SEM), and photoluminescence (PL) spectroscopy. The band gap ...

An automated micromethod for measuring iron concentration in serum employing thioglycollic acid and bathophenantroline sulphonate as reducing agent and chromogen respectively, is described. Measurements are carried out using an AutoAnalyzer (Technicon) and require 0.1 ml of sample. The reproducibility, assessed by the mean coefficient of variation (1.9%), and the mean recovery of iron added to ...

A series of 2-(p-substituted benzylidene)-3-(5-ethyl-1, 3, 4-thiadiazol-2-yl) thiazolidin-4-ones were synthesized by the reaction of Schiff’s bases of N-(p-substituted benzylidene)-5-ethyl-1, 3, 4-thiadiazole-2-amines with thioglycolic acid in 1, 4-dioxane as solvent and studied for their in vitro antibacterial activity. Reaction of thiosemicarbazide with propanoic acid in presence of concentra...

An improved method for determination of Mo by thiocyanate has been standardized by employing thioglycollic acid, instead of currently employed stannous chloride, as reductant of Mo. The method ensures stability of the colored complex in aqueous acidic medium for about 3.5 hours which is otherwise unachievable and the color unstable while using stannous chloride. The method is linear over 0.5 to...

1. Group A streptococci sometimes produce in broth culture an extracellular proteolytic enzyme. 2. Under suitable cultural conditions the enzyme has been demonstrated in representative cultures of most of the Griffith types. Its production by a given strain may be suppressed by serial passage through mice and the variant so produced has been found to maintain this change in character on subcult...

Since the discovery of glutathione (16), many workers have demonstrated its occurrence and the significant role of sulfhydryl groups in growing tissues and organisms (13, 17, @4). More recently, the studies of Hellerman et al. (14), Rapkine (@3), and Barron et al. (1, 3) have emphasized the im portance of -SH groups in enzyme systems. Bar ron et al. (1) found that small amounts of x-radia tion ...