Hydrogen peroxide as an oxidant agent was used for desulfurization of a petroleum hydrocarbon fraction (C10-C22) with boiling range of 175-375 ℃, (light fuel oil) in the presence of acetic acid as catalyst. The oxidation was performed in an ultrasonic bath. It is found that increasing the amount of hydrogen peroxide lead to increase the oxidation rate and so desulfurizatio...

mixed-addenda vanadium substituted polyoxometalate supported on anatase tio2 crushed nano leaf was synthesized by an unusual reaction with titanium tetraisopropoxide at 100 ºc via sol–gel method under oil-bath condition. the materials characterized by xrd, tem,  ir and uv–vis  techniques.  in  the  present  work,  efficient  oxidative  of  thiols  with  polyoxometalate-tio2/hydrogen  peroxide  ...

In this paper, the polyphenol content and antioxidant activity of fig leaf extracts were analyzed. Extraction was performed with methanol, ethanol, acetone their aqueous mixtures (50:50 v/v). Extractions stirring at 300 rpm on a vibromix ultrasonic bath for 15 minutes. The determined spectrophotometrically using Folin-Ciocalteu test. Antioxidant capacity tested FRAP DPPH methods. results showed...

In this article, we combine the homophase junction g-C3N4 prepared by recrystallization with small particles of MoS2 treated ball milling through a simple method ultrasonic assisted oil bath, which improves light absorption capacity catalyst and promotes electron transport separation efficiency electrons, photocatalyst capable efficiently degrading pollutants was prepared.

A perfluorocarbon nanodroplet formulation is shown to be an effective cavitation enhancement agent, enabling rapid and consistent fragmentation of genomic DNA in a standard ultrasonic water bath. This nanodroplet-enhanced method produces genomic DNA libraries and next-generation sequencing results indistinguishable from DNA samples fragmented in dedicated commercial acoustic sonication equipmen...

Ultrafiltration (UF) of whey is a major membrane based process in the dairy industry. However, commercialization of this application has been limited by membrane fouling, which has a detrimental influence on the permeation rate. There are a number of different chemical and physical cleaning methods currently used for cleaning a fouled membrane. It has been suggested that the cleaning frequency ...

Mixed-addenda vanadium substituted polyoxometalate supported on anatase TiO2 crushed nano leaf was synthesized by an unusual reaction with titanium tetraisopropoxide at 100 ºC via sol–gel method under oil-bath condition. The materials characterized by XRD, TEM,  IR and UV–vis  techniques.  In  the  present  work,  efficient  oxidative  of  thiols  with  polyoxometalate-TiO2/hydrogen  peroxide  ...

The cleaning of heat exchangers, and other large process equipment, using large-scale ultrasonic systems has, in the past few years, progressed from a “curiosity” to a proven, practical tool for many clients. Research and a greater understanding of the physics involved in the cleaning process and the practical considerations of operating in the field have led to improvements in design and usabi...

Kleinová J., Klejdus B. (2014): Determination of volatiles in beer using solid-phase microextraction in combination with gas chromatography/mass spectrometry. Czech J: Food Sci., 32: 241–248. Headspace solid phase microextraction and purge and trap analysis were used for the determination of volatiles in beer. These methods were compared with the analysis of unconcentrated gas phase and liquid ...

Present study aims the optimisation and validation of the extraction procedures for the determination of polycyclic aromatic hydrocarbons (PAHs) in sediment samples. As analytical techniques, gas chromatographymass detector (GC-MS) and gas chromatography-flame ionization detector (GC-FID). The optimized methods were soxhlet extraction, ultrasonic bath extraction and solid phase micro extraction...