In this research, calcium titanate nanoparticles have been synthesized via mechanical alloying (MA). By changing the parameters of mechanical alloying, optimal conditions for synthesis of this compound was determined. For synthesis of this compound, a mixture of calcium hydroxide and titanium dioxide, rotation speed of 250 rpm and differnet ball to powder weight ratio was used. Phase investigat...

This research report related to nano-sized particles of tetragonal rutile phase TiO2. We havesuccessfully synthesized TiO2 nanoparticles, by chemical method non-toxic and bio-safe, at lower than 100°C. This method is simple, economic and friendly for environmentally and suitable for large scale grains. Using of choline chloride, to decrease the size of commercial TiO2 by chemical method. ...

Mn doped ZnO nanocrystals were prepared by co-precipitation route sintered at 450 °C temperature. XRD results indicate that the samples having hexagonal (wurtzite) structure. From X-ray data it is found that the lattice parameters increase with increasing Mn concentration. The X-ray density decreases with increasing Mn concentration of Zn 1-x Mnx O nanocrystals. It indicates that the Mn...

Numerous experiments have shown that strain broadening caused by dislocations can be well described by a special logarithmic series expansion of the Fourier coefficients of Bragg reflection peak profiles. In the present work it will be shown that this formalism can be incorporated into the classical methods of Williamson-Hall and Warren-Averbach. The new procedures are suggested to be called mo...

In this article, some Fe (III) doped hydroxyapatite samples (FeHAp) were prepared using the wet chemical method. The prepared samples were characterized via the use of X-ray diffraction (XRD) and scanning electron microscopy (SEM). Detailed structural analysis were done by Scherrer and Williamson–Hall plot methods to detect the effect of iron on the structure of hydroxyapatite (HAp). XRD patter...

Worm-like nanorods and nanospheres of silver have been synthesized by photochemical decomposition of silver oxalate in water by UV irradiation in the presence of CTAB and PVP, respectively. No external seeds have been employed for the synthesis of Ag nanorods. The synthesized Ag colloids have been characterized by UV-visible spectra, powder XRD, HRTEM, and selected area electron diffraction (SA...

Present work reports the synthesis of RE3+ (La3+, and Ce3+) Co2+ co-doped Zn0.75Cu0.25Fe2O4 samples powder using sol-gel auto combustion process. Rietveld refinement established spinel matrix with space group (F d -3 m) suggests that uniform distribution cations at tetrahedral octahedral lattice sites. The comparative study crystallite size (D) was found Scherrer's relation, plot, Williamson-Ha...