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Four commonly applied extraction techniques for organochlorine pesticides, microwave-assisted extraction (MAE), accelerated solvent extraction (ASE), quick, easy, cheap, effective, rugged, and safe (QuEChERS) extraction and ultrasonic solvent extraction, were applied on soil samples in order to evaluate their performances. The extracts were analyzed by GC-ECD and confirmed by GC-MS/MS. The MAE ...

Effects of varying temperatures with constant pressure of solvent on extraction efficiency of two chemically different alkaloids were studied. Camptothecin (CPT) from stem of Nothapodytes nimmoniana (Grah.) Mabb. and piperine from the fruits of Piper nigrum L. were extracted using Accelerated Solvent Extractor (ASE). Three cycles of extraction for a particular sample cell at a given temperature...

The efficient extraction of phenols from grapes is an important step for their reliable quantification. aim was to optimise the lyophilisation process and grape skins seeds. phenol yield lyophilised tissues investigated with different accelerated solvent (ASE) operating conditions. Skins seeds were separated frozen berries without being ground. weight loss during followed daily. Phenols extract...

The present study is aimed to examine and compare the storage stability of seed kils extracted form red pepper (Capsicum annuum L.) waste by green techniques (cold pressing, ethanol solvent, ultrasound-assisted solvent extraction). In accordance with this purpose, oil samples were stored for a period 6 weeks at 60°C under accelerated conditions analyzed weekly intervals peroxide, conjugated die...

IntroductIon The presence of polychlorinated biphenyls (PCBs) in fish and other marine organisms is of immediate environmental and regulatory concern. To determine the concentrations of PCBs indicative of contaminant exposure, and lipids, which also characterize physiological conditions of fish, the analytes must first be extracted. Traditionally, this has been done using Soxhlet methods that a...

An extraction technique is described for vitamin K1 in medical foods, using accelerated solvent extraction (ASE) in conjunction with matrix solid-phase dispersion (MSPD). The medical food sample is treated as it would be with MSPD extraction, followed by ASE for a hands-free automated extraction. The vitamin K1 in the ASE extract is then quantitated by reversed-phase liquid chromatography with ...

This paper describes a comparative study of extraction methods of terpenes (terpenic alcohols and phytosterols), fatty acids and Vitamin E from leaves of Piper gaudichaudianum Kunth. The analysis of extracts was done by gas chromatography with mass spectrometric detection. The identification and quantification was made by co-injections of the extract with certified standards. The use of pressur...