A simple, efficient and cost effective method was developed and optimized for the digestion of fish tissue for the determination of Lead, Cadmium, Mercury, Antimony, Arsenic and Selenium by FAAS, CVAAS and HGAAS. Three of the more common classical open tubed acid digestion procedures were explored with the purpose of optimizing the variables and selecting the single most efficient, convenient a...

This paper presents a comparative description of different methods of determination of arsenic, antimony and selenium: spectrophotometric, electro-analytical (voltamperometry), activation analysis, atomic fluorescence and the methods of inductive or microwave-induced plasma in combination with different detection methods (emission or mass spectrometry). The description is based on literature da...

This paper presents results of the determination of the total concentration of arsenic, antimony and selenium and their inorganic speciation forms in water samples from grate ashes dumping grounds. Determined concentrations of elements were up to 128.8 ng/mL for arsenic, 153.7 ng/mL for antimony and 52.9 ng/mL for selenium, at the detection limits of 0.16 ng/mL for As, 0.18 ng/mL for Sb and 0.1...

BACKGROUND Treatment-refractory visceral leishmaniasis (VL) has become an important problem in many countries. OBJECTIVES We evaluated the antimony-resistance mechanisms of Leishmania infantum isolated from VL patients refractory or responsive to treatment with pentavalent antimony. METHODS Strains isolated from antimony-refractory patients (in vitro antimony-resistant isolates) and antimony-re...

Anewphase of antimony(V) phosphate has been synthesizedand characterized usingX-ray, JR, SEM, TGA and DTG studies in addition to ion exchange studies such as determination of ion exchangecapacity, e1ution,pH titration and distribution behaviour. On the basis of the distribution behaviour, the material has been found to behighly selectivefor lead. Somebinary separationsofmetal ionshavealso beenp...

Vortex-assisted surfactant-enhanced emulsification microextraction based on solidification of floating organic drop (VASEME-SFO) was used for preconcentration and speciation of antimony (ΙΙΙ, V) followed by electrothermal atomic absorption spectrometry (ETAAS). In this procedure, Triton X-114 was used as emulsifier and 1-undecanol was used as extraction solvent. This method is based on the comp...

Until ten years ago the grids of lead-acid batteries were usually made of lead-antimony alloys containing 5-11 wt. % antimony. The necessary mechanical strength and castability are easily achieved with this content of antimony. However, the unavoidable corrosion of the positive grid liberates antimony from the grid, which proves to be both unfavorable as well as unfavorable with respect to batt...