It has recently been shown that Severe Plastic Deformation (SPD) techniques could be used to obtain nanostructured metal hydrides with enhanced hydrogen sorption properties. In this paper we review the different SPD techniques used on metal hydrides and present some specific cases of the effect of cold rolling on the hydrogen storage properties and crystal structure of various types of metal hy...

Mechanical alloying (MA) is a solid-state powder processing technique involving repeated cold welding and fracturing of powder particles in a high-energy ball mill. It has been used to obtain nanocrystalline binary system FeNi. Fe and Ni elemental powders have been ball milled in a planetary mill (Pulverisette5, Fritsch) for various times up to several hours. The morphology of the powders was e...

The effect of ball-milling on physicochemical properties of maize starch was evaluated. Results found that the cold water solubility (CWS) of maize starch was positively correlated with the time of milling up to 3 h. There was no significant influence of using a ceramic pot versus a stainless steel pot on CWS. However, following 5 h of ball-milling CWS increased quite dramatically in the cerami...

Anatase-to-rutile phase transformation was studied in milled and unmilled samples. Ball milling was carried out in two types of ball mills, planetary and tumbler, with a ball-to-powder ratio of 40:1 over 2-48 hours. First, the unmilled samples were heated in the furnace at various temperatures for different periods of time. The results revealed that the anatase-to-rutile transformation comple...

One of the principal problems with nano-crystalline materials is producing them in quantities and sizes large enough for valid mechanical property evaluation. The purpose of this study was to explore an innovative method for producing nano-crystalline γ-TiAl bulk materials using high energy ball milling and brief secondary processes. Nano-crystalline powder feedstock was produced using a Fritsc...

High-density fine-grained Ni0.5Zn0.5Fe2O4 ferrite ceramics were synthesized by spark plasma sintering (SPS) in conjunction with high energy ball milling. The precursor powders were milled for 20 h, 40 h, and 60 h, respectively, and the milled powders were all sintered for 5 min at 900 ̊C. All the samples exhibit a single spinel phase. With increasing of the ball milling time, the relative densit...

This work studied the benefits of adding different enzyme cocktails (cellulase, xylanase, β-glucosidase) to pretreated switchgrass. Pretreatment methods included ammonia fiber expansion (AFEX), dilute-acid (DA), liquid hot water (LHW), lime, lime+ball-milling, soaking in aqueous ammonia (SAA), and sulfur dioxide (SO(2)). The compositions of the pretreated materials were analyzed and showed a st...

This paper introduces a method to determine the tool wear by measured cutting force in Ball-nose End Milling. The features will be extracted from the measured cutting force with different flank wear. As the adaptive window width in wavelet transform is an advantage for analyzing and monitoring the rapid transient of small amplitude of cutting force signals when cutting engagement changes along ...

The effects of plastic deformation by ball milling on the structure of a partly amorphousAl87Ni8La5alloy were investigated by X-ray diffractometry. Lattice parameter, crystallite size and lattice strain of the fcc-Al precipitates were determined by Rietveld refinement, doubleVoigt approach and Williamson-Hall plots. The changes in lattice parameter of fcc-Al nanoprecipitates during ball milling...

The chatter is one of the major limitations of the productivity in the ball end milling process. It affects the surface roughness, the dimensional accuracy and the tool life. The aim of this research is to propose the new system to detect the chatter during the ball end milling process by using the wavelet transform. The proposed method is implemented on the 5-axis CNC machining center and the ...