Calcium doped nickel ferrite powders have been prepared by sol-gel combustion technique. Metal nitrates, such as calcium nitrate, nickel nitrate and ferric nitrate, were used as the source materials and citric acid and polyvinyl alcohol were used as the burning agent and agglomeration reducing agent, respectively. The average crystallite size of the prepared ferrite was in the order of ~70- 92 ...

Abstract: Auto-ignited gel combustion process has been used for producing a red hematite-zircon based pigment. The combustible mixtures contained the metal nitrates and citric acid as oxidizers and fuel, respectively. Sodium silicate (water glass) was used as silica source for producing zircon phase. X-Ray Diffractometery, Electron Microscopy and Simultaneous Thermal Analysis were used for ...

background: summer savory (satureja hortensis l.) is one of the most important medicinal and spice plants cultivated in many parts of the world. objective: a greenhouse experiment was conducted to study the effects of feso4 and citric acid application on the morphological traits and essential oil content and its component, gamma-terpinene in s. hortensis. methods: feso4 in four levels (0, 3, 4 ...

Development of methodology for the recovery of citric acid from the fermented broth involves standardization of the various parameters to achieve maximum performance in terms of recovery and optimum conditions. The present investigation was carried out to study the purification of citric acid from fermented broth by calcium carbonate precipitation and subsequent acid hydrolysis. The parameters ...

Citric acid is the most widely used organic acid in the field of foods and beverages as an acidulant as well as in pharmaceutical and chemical products. Generally, surface or submerged fungal fermentation mainly with aspergillus niger is utilized for citric acid production. However, the submerged fermentation method is the most used method for citric acid production.1,2 The method of calcium sa...

Copolymers of citric acid and D-sorbitol were synthesized with a solventfree vacuum-oven synthesis with molar ratios of citric acid to D-sorbitol ranging from 1/1 to 6/1. The extent of the reaction was followed by the monitoring of the residual acid content of the system. As expected, the reaction occurred much more rapidly at 150 than at 110 8C. The Fourier transform infrared (FTIR) spectra of...

Citric acid is a regular ingredient in many vase solution formulations but pre-harvest use of citric acid is a novel method in vase life extension of cut flowers, which is reported on tuberose earlier. In order to verify previous result, and check for possible substitution of citric acid by malic acid, the current research was designed. Citric acid (0, 0.075, 0.15% w/v) and malic acid (0, 0.075...

Nano-crystalline TiO2 were synthesized by combustion method using metal nitrate solution and urea, glycin and citric acid fuels. Microwave irradiation was used as heating source. X-ray diffraction, scanning electron microscope as well as Fourier transform infrared spectroscopy were performed to characterize the obtained samples. X-ray diffraction patterns revealed that in the case of citric aci...

In this study, nanosilica particles were prepared from self-made silica gel under the protection of citric acid in situ complexation and ethyl acetate as latent reagent. The effects acetate, acid, reaction temperature, time on particle size studied. optimum process parameters determined follows: Vethyl acetate: Vsilica sol = 9:50, addition amount 3.64%, 8 h, temperature 70 °C. products characte...

stoichiometric tetragonal bal-xsrxtio3 (x = 0.23) nanopowders were prepared by stearic acid gel(sag) method using barium stearate, strontium stearate, tetrabutyl titanate as ba, sr, ti sourcesand stearic acid as complexing reagent. thermal analysis including differential thermogravimetric(dtg) and tg, fourier transform infrared spectrometry (ftir), x-ray diffraction (xrd) andtransmission electr...