Distillation columns have been widely used in chemical plants for separation process. The high nonlinearity and dynamic behavior of the column make them hard to control. Internal Model Control (IMC) is one of the model based control strategy that have become the central of research to control such column. This paper will review the implementation of IMC in controlling continuous distillation co...

In this contribution, a different pressure thermally coupled extractive distillation process has been applied on the separation of propylene and propane with aqueous acetonitrile (ACN) solution as entrainer. The novel distillation process integration is the combination of different pressure thermally coupled distillation (DPTCD) and extractive distillation (ED). Both the new process and the con...

Extractive distillation is an alternative for ethanol dehydration processes that has been shown to be more effective than azeotropic distillation and, in close proximity, to be very competitive against the process that uses adsorption with molecular sieves. Glycols have been shown to be the most effective solvents in extractive distillation, mainly ethylene glycol and glycerol. In this work, an...

INTRODUCTION In Japan, Pilot Plant of the HIDiC was built in 2005. It was commercial base scale and already achieved the consecutive distillation for 1000 hours. The energy consumption of the pilot HIDiC was only about 70% of that of a conventional distillation column. The HIDiC can lower reboiler and condenser load by heat exchange between rectifying section and stripping section. Therefore, i...

Reactive distillation is an excellent example of recent advances in process intensification. It combines reaction and separation operations in one piece of equipment. This paper studies the steady-state economic optimum design of a chemical process with a generic exothermic reversible reaction A+B↔C+D for two different process flowsheets: a conventional multi-unit reactor/separator/recycle stru...

Distillation Residue Curve Maps (D-RCM’s) have proven to be an extremely useful graphical tool in the design and operation of both batch and continuous distillation processes. Recently submitted work by the authors has investigated the applications of Residue Curve Maps for membrane permeation systems. Such maps are referred to as M-RCM’s. This paper aims to develop a graphical tool to provide ...

HYSYS process modeling software was used to analyze the effect of reflux ratio and number of trays on the purity of ethylene in a vapor recompression distillation column and also in an ordinary distillation column. Analysis of data showed that with increased pressure a higher reflux ratio is needed to obtain a purity of 99.9% for both towers. In addition number of trays was varied to see its ef...

Distillation has remained an important separation technology for the chemical process industries. In 1997 it was reported in the journal Chemical Engineering that about 95% of all worldwide separation processes use this technology. In the USA alone, some 40000 distillation columns represent a capital investment of about US $8 billion. They consume the energy equivalent of approximately 1 billio...

Batch distillation in a column with a middle vessel can avoid many of the disadvantages associated with the regular batch distillation processes. In this paper we present an experimental investigation of the separation of a zeotropic ternary mixture via total reflux operation and of the separation of an azeotropic binary mixture via batchwise extractive distillation. Moreover, the results obtai...