a column of alumina modified with sodium dodecyl sulfate (sds) and dimethylglyoxime (dmg) was prepared for the preconcentration of trace nickel from water samples for flame atomic absorption spectrometry (faas) determinations. under optimized conditions (ph=7.0; flow rate: 20 mlmin-1) nickel was retained on the column. the nickel collected on the column was eluted with 5 ml of 1 m nitric acid. ...

a simple, sensitive and accurate method for spectrophotometric determination of dalacinphosphatehas been established. the method is based on the reduction of atomic absorptioncalcium ion by phosphate. because, there is a phosphate mole in every dalacin mole structureand with measurement of phosphate, dalacin is beyond measurement too. therefore, the reactionbetween acidic hydrolysis products of...

In this work a rapid and selective procedure for separation and preconcentration of lead(Pb2+) before determination by electrothermal atomic absorption spectrometry (ETAAS) wasdeveloped. The procedure is based on the electrodeposition on a graphite probe modified withpalladium. The lead was deposited from acetate buffer solution at pH 5.5. Various parameters,such as pH of solutions, deposition ...

in the present study, the concentrations of three heavy metals including lead (pb), zinc (zn) and arsenic (as) in 72 different honey samples collected from north-western regions of iran were investigated using atomic absorption spectroscopy method. all metals were detected in 88.88% of the honey samples. the range of metals contamination in honey samples was 0.01 to 11.09 ppm. zn was the most a...

in this study, 60 composite samples of dill and onion from two different cultivated areas in khozestan province, iran, were collected and analyzed for the presence and determination of lead and cadmium by flame atomic absorption spectrometry. samples were burned according to aoac at 450 °c, and the residue was dissolved in nitric acid. lead and cadmium contents were determined using calibration...

a new method for the determination of trace copper(ii) in food samples by cloud point extraction(cpe) combined with flame atomic absorption spectrometry(faas) is presented and evaluated. the method is based on the fact that hydrophobic complex of copper(ii) with sodium diethyldithiocarbamate (ddtc) was formed at ph 6.0 and subsequently the hydrophobic complex was extracted into surfactant-rich ...