Combination of the surfactant-free nonaqueous sol–gel approach with the microwave technique makes it possible to synthesize Fe3O4, CoFe2O4, MnFe2O4, and NiFe2O4 nanoparticles of about 5–6 nm and with high crystallinity and good morphological uniformity. The synthesis involves the reaction of metal acetates or acetylacetonates as precursors with benzyl alcohol at 170 C under microwave irradiatio...

Magnetic nanoparticles of cobalt ferrite (CoFe204) have been synthesized using water-in-oil microemulsions consisting of water, cetyl trimethyl ammonium bromide (surfactant), n-butanol (cosurfactant), and n-octane (oil). Precursor hydroxides were precipitated in the aqueous cores of water-in-oil microemulsions and these were then separated and calcined to give the magnetic oxide. X-ray diffract...

We report a novel core-shell-structured ternary nanocube of MnZn ferrite synthesized by controlling the reaction temperature and composition in the absence of conventionally used reducing agents. The highly monodispersed core-shell structure consists of an Fe(3)O(4) core and an MnZn Ferrite shell. The observation of a Moiré pattern indicates that the core and the shell are two highly crystallin...

Lanthanum substituted Ni-Zn ferrite nanoparticles (Ni0.5Zn0.5LaxFe1-xO4; 0.00 ≤x≤ 1.00) synthesized by sol-gel method were presented. X-ray diffraction patterns reveal the typical single phase spinel cubic ferrite structure, with the traces of secondary phase for lanthanum substituted nanocrystals. In addition, the structural analysis also demonstrates that the average crystallite size varied i...

In this research nickel zinc ferrite nanoparticles with composition of Ni1-xZnxFe2O4 (where x=0, 0.3, 0.7, 1) were synthesized by a sol-gel method at 600 °C for 5 hours. The structure of nanoparticles was studied using X-ray diffraction pattern. The lattice parameter of ferrite nanoparticles was calculated and indicates lattice constant of nanoparticl...

NiFe₂O₄ and ZnFe₂O₄ nanoparticles have been prepared encased in the MCM (Mobile Composition of Matter) type matrix. Their magnetic behavior has been studied and compared with that corresponding to particles of the same composition and of a similar size (prepared and embedded in amorphous silica or as bare particles). This study has allowed elucidation of the role exerted by the matrix and inter...

Cobalt ferrite nanoparticles were synthesized with coprecipitation or with the hydrothermal method. Stable water suspensions were prepared from the as-synthesized nanoparticles, with the addition of citric acid as a surfactant, and then used for the preparation of deposits under an applied magnetic field. The morphology of the cobalt ferrite nanoparticles was investigated with a transmission el...

The contact of a steel electrode with water dispersion medium in an open-air system leads to the development of various polymorphic iron oxides and oxyhydroxides on the steel surface. Whereas the usage of distilled water causes the obtaining of Fe(II)-Fe(III) layered double hydroxides (green rust) as a primary mineral phase, but in the presence of inorganic 3d-metal water salt solutions, mixed ...

BACKGROUND Nickel ferrite, a kind of soft magnetic materials is one of the most attracting class of materials due to its interesting and important properties and has many technical applications, such as in catalysis, sensors and so on. In this paper the synthesis of NiFe2O4 nanoparticles by the hydrothermal method is reported and the inhibition of surfactant (Glycerol or Sodium dodecyl sulfate)...

hard magnetic srfe12o19 (srm) nanoparticles were synthesized by a facile sonochemical reaction. the magnetic nanoparticles were then added to acrylonitrile-butadiene-styrene, polystyrene, polycarbonate, and poly sulfone to make magnetic nanocomposites. the magnetic properties of the samples were also investigated using an alternating gradient force magnetometer. the strontium ferrite nanopartic...