The present research attempt consists in the development of mesoporous hydroxyapatite using inexpensive ingredients using cetyltrimethylammonium bromide (CTAB) as template through a chemical-based hydrothermal method. Wide angle X-ray diffraction (XRD) reveals the formation of pure single-phased hydroxyapatite particles. Fourier transform infrared absorption spectroscopy (FTIR) and electron dif...

A novel metal-organic framework assembled from Y(iii), Li(i), and terephthalate ligand, formulated as [LiY(BDC)2(H2O)·2(H2O)] (1) (H2BDC = terephthalic acid), has been obtained as single phase under hydrothermal conditions. The crystal structure was solved by single-crystal X-ray diffraction and the bulk was characterized by powder X-ray diffraction (PXRD), thermal analyses (TG-MS and DSC), vib...

We investigate the effect of synthesized time on the structure, as well as optical properties in ZnWO4 nano rod prepared by hydrothermal method. The prepared rods were characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM), Raman scattering, absorption and photoluminescent (PL) spectra techniques. The size and morphology of ZnWO4 nano-rod can be controlled by adjusting the...

PbO nanoparticles were synthesized using hydrothermal process. Scanning electron microscopy (SEM) was used in order to investigate of PbO powders. X-ray diffraction (XRD) pattern confirmed β-PbO formation during this process. The crystallite size of the powders was calculated using Scherrer formula about 74.6 nm. Electrochemical evaluation of the PbO nanoparticles as anode for Li-ion batteries ...

in this study, pyrite was produced by hydrothermal precipitation from the reaction between feso4 and na2s2o3 at high pressure and high temperature in a stirred reactor. the solid product was purified by means of solvent extraction to remove sulfur. powder was characterized by x-ray diffraction (xrd), scanning electron microscopy (sem) and thermal analyses. results indicated that pyrite was prod...

in this paper, indium tin oxide (ito) nanoparticles has been prepared by chemical methods under given conditions with solution of indium chloride (incl3·4h2o), tin chloride (sncl4·5h2o) in ammonia solution. the samples were characterized by x-ray diffraction (xrd) and scanning electron microscopy (sem) analyses after heat treatments. the sem results showed that, the size of the ito particles pr...

Bismuth oxide (Bi2O3) nanorods was prepared via one pot sol-gel method using Bi(NO3)3.5H2O and starch (as template) in water under hydrothermal condition followed by calcination at 320˚C within 3 h. The resultant solid product was characterized by scanning electron microscope (SEM), X-ray diffraction (XRD), thermogravimetry (TGA), and FTIR techniques. Based on the obtained results, the formatio...

the preparation of nano-sized tio2 by titanium tetraisopropoxide (ti(oipr)4) via sol-gelmethod using acid as a catalyst is investigated and the optimized conditions concerning theproportional amount of acid, water, alcohol is established by xrd and sem. the effect ofcalcination temperature on phase transformation of tio2 (rutile, anatase and brookite) wasdetermined by xrd. the smallest grain si...

Gapped hollow BaTiO3 nanospheres with an apparent diameter of 93 ± 19 nm (shell thickness of 10-20 nm) were synthesized via a dynamic hydrothermal process using TiO2 sols and Ba(2+) ions as the Ti and Ba sources in alkaline aqueous solutions. The phases and morphologies of the BaTiO3 samples were characterized by X-ray diffraction (XRD), SEM, TEM, and Raman spectra. The effects of the hydrother...

In this study, carbon nano-micro spheres with tightly controllable size, regular and perfect shape, high yields and narrow size distribution were prepared simply from glucose and DI water as precursors using a hydrothermal method. By setting the initial concentration of glucose solution and changing the hydrothermal process time at a constant temperature of 160 °C, carbon spheres with various s...