This study investigates the influence of microstructure on the effective ionic and electrical conductivities of Ni-YSZ (yttria-stabilized zirconia) anodes. Fine, medium, and coarse microstructures are exposed to redox cycling at 950 °C. FIB (focused ion beam)-tomography and image analysis are used to quantify the effective (connected) volume fraction (Φeff), constriction factor (β), and tortuos...

The influence of B203 on the microshucture and magnetic properties of pure Mn-Zn ferrites has been investigated. A citrate gel processing route was employed to produce highly homogeneous Mn-Zn (MQ,~,Z~.,F~,,OJ ferrites undoped or doped with B203 (0-2.5wt%). The results show that B203 doping does not benefit the magnetic properties of these femtes, but promoted grain growth significantly. The in...

in this article, commercially pure copper samples were severely deformed by equal channel angular pressing (ecap) up to eight passes at room temperature. the effects of severe plastic deformation on the microstructure, mechanical properties, and electrical conductivity of the copper were investigated. the microstructure evolution was followed by optical microscope and field emission scanning el...

Austenitization is an inevitable occurrence during the heat treatment of steels. Despite this consideration, less attention has been paid so far to the study of the formation of austenite as compared with the vast amount of research on its decomposition. That is because the steel properties depend basically on the transformation processes following austenitization. However, the initial austenit...

Abstract:Optimization of specimen geometry before subjecting it to hot torsion test (HTT) is essential for minimizingnon-uniform temperature distribution and obtaining uniform microstructure thought the specimen.In the present study, a nonlinear transient analysis was performed for a number of different geometries andtemperatures using the commercial finite element (FE) package ANSYSTM. FE ther...

the effect of secondary steelmaking processes such as desulphurization, removal of inclusions and vacuumdegassing followed by hot forging and hardening heat treatment on the microstructure and mechanical properties of a hot-work w500 tool steel have been studied in details. in order to follow the progress of secondary steel making, the content of impurity elements such as s, p, o, h and n were ...

In this paper, a 0.2 C–1.6 Mn–1.5 Si wt. % TRIP-aided cold-rolled steel sheet was fabricated and the optimal heat treatment conditions (Intercritical Annealing “IA” and Bainitic Isothermal Transformation “BIT”) were investigated to maximize the volume fraction and stability of the retained austenite. The effects of temperature on IA (770, 790 and 810 ºC) and BIT (330, 350 and 370 <su...

A review on the microstructural evolution in magnesium alloys during severe plastic deformation waspresented. The challenges deserved to achieve ultrafine/ nanostructured magnesium were discussed.The characteristics of the processed materials are influenced by three main factors, including i)difficult processing at low temperatures, ii) high temperature processing and the occurrence ofdynamic r...

The effects of initial twinned microstructure on the grain growth behavior four sputtered nanotwinned copper alloys were compared. As-deposited films characterized by transmission electron microscopy and microstructural evolution annealed samples was investigated through backscatter diffraction. Texture showed a pronounced effect, where with strong {111} textures exhibited abnormal that not obs...