a simple, rapid and sensitive solvent assisted-dispersive solid phase extraction method was developed for the extraction of iron(ii) prior to its spectrophotometric determination. the fe(ii) reacted with 2,4,6-tris(2-pyridyl)-1,3,5-triazine, neutralized with sodium dodecyl sulfate and extracted onto the fine particles of benzophenone which were formed upon rapid injection of a mixture of benzop...

Polyaniline/Fe3 O4 magnetic nanoparticles were synthesized and employed as a sorbent for the magnetic solid phase extraction (MSPE) of seven triazine herbicides from environmental water samples. The properties of the prepared magnetic sorbent were characterized using field emission-scanning electron microscopy (FE-SEM), fourier transform infrared spectroscopy (FT-IR), vibrating sample magnetome...

A facile method for synthesis of amino functionalized silica coated Fe3O4 magnetic nanoparticles is introduced. For this purpose, the surface of magnetic nanoparticles (MNPs) was modified with two precursors of silica which produced amine and vinyl functional groups on the surface of magnetic nanoparticles. The modified magnetic nanoparticles were characterized by transmission electron micr...

Objective(s):The present study reports the development and validation of a sensitive and rapid extraction method beside high performance liquid chromatographic method for the determination of crocetin in human serum. Materials and Methods:The HPLC method was carried out by using a C18 reversed-phase column and a mobile phase composed of methanol/water/acetic acid (85:14.5:0.5 v/v/v) at the flow...

This review aimed to inform about the magnetic nanoparticle functionalization and solid phase extraction application separate analytes in various types of samples. The was conducted by analyzing several articles published 2010 until 2021 obtained through search engines, such as Science Direct, Google Scholar PubMed, using keyword “magnetic extraction” nanoparticle”. can be functionalized with o...

The magnetic aqueous micellar two-phase system (MAMTPS) has the advantages combined of magnetic solid phase extraction (MSPE) and aqueous micellar two-phase system (AMTPS). Thus, MAMTPS based on Fe3O4 magnetic nanoparticles (MNPs) and a nonionic surfactant Triton X-114 (TX-114) was developed for the extraction, enrichment and removal of three dyes (Congo red, methyl blue, and methyl violet) fro...

background & aim:nepeta racemosa is an herbal and medicinal plant and this report aims to   identify chemical compositions of the essential oils and volatiles of its   aerial parts through classical and advanced methods.  experimental: chemical profiles of the essential oils and volatile compounds from the aerial parts of nepeta racemosa obtained through hydrodistillation (hd), solvent-free mic...

In this paper, magnetically multiwalled carbon nanotubes (MMWCNTs) nanocomposite modified by methyl-2-[2-(2-2-[2-(methoxycarbonyl) phenoxy] ethoxyethoxy) ethoxy] benzoate was applied for magnetic solid-phase extraction (MSPE) of thallium(I) ions. Fourier transform infrared (FT-IR) spectroscopy, field emission scanning electron microscopy (FE-SEM), X-ray diffraction (XRD) spectrometry and vibrat...

A simple, highly sensitive, accurate and selective method for determination of trace amounts of Ni2+ in water samples. In this paper, Dioctylphthalate (DOP) was used to encapsulate nano-Fe3O4 and produce a nano-Fe3O4-DOP sorbent based new sorbent was prepared. This was treated with ethylenediamine (ED) in another solvent-free procedure for the formation of a novel nano-Fe3O4-DOP-ED. Flame atomi...