نتایج جستجو برای: nmr analysis

تعداد نتایج: 2869644  

Journal: :journal of sciences islamic republic of iran 0

a new homologous series of linear aliphatic polyesters, such as poly (cis-2- butenylene carboxylate)s, pbms (m is the number of methylene groups in the acid component, m=2-8 have been synthesized by direct polyesterification reactions in anisole, as solvent. ft-ir, 400 mhz h- nmr, c-nmr and elemental analysis were used to establish the structure of polyesters. molecular weight distributions wer...

Journal: :Clinica chimica acta; international journal of clinical chemistry 2017
Marc Cassiède Sindhu Nair Meghan Dueck James Mino Ryan McKay Pascal Mercier Bernadette Quémerais Paige Lacy

BACKGROUND Proton nuclear magnetic resonance (1H NMR, or NMR) spectroscopy and inductively coupled plasma-mass spectrometry (ICP-MS) are commonly used for metabolomics and metal analysis in urine samples. However, creatinine quantification by NMR for the purpose of normalization of urinary metals has not been validated. We assessed the validity of using NMR analysis for creatinine quantificatio...

Journal: :Journal of Physics: Conference Series 2016

Journal: :iranian chemical communication 2016
reza golbedaghi ehsan alavipour

in this paper, we report the synthesis and characterization of a new symmetric macroacyclic schiff base ligand (h2l) and related complexes with different metals. (h2l) was synthesized by the one pot condensation reaction of 2-[2-(2-formyl phenoxy)ethoxy]benzaldehyde and 2-aminobenzenethiol in a 1:2 molar ratio. the acyclic schiff base was characterized by ir, nmr spectroscopy and elemental anal...

Journal: :iranian journal of chemistry and chemical engineering (ijcce) 1998
javad sabounchei sadegh salehzadeh

195pt and 1h nmr has been used to show that addition of chlorine and bromine to [pt(cn)4]2_ in presence of perchloric acid in water results in cyanide and water scrambling with formation of eleven complexes of the type [pt(cn)4-ncl(h2o)n+1](n-1)+ (n=0, 1, 2, 3, 4). addition of nbu4oh to this solution gives (nbu4)2[pt(cn)4cl(oh)]. nmr measurements in acetone also show cyanide and hydroxyl group ...

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