Simple, accurate and precise spectroflourometric and spectrophotometric methods have been developed and validated for the determination of sitagliptin phosphate monohydrate (STG) and metformin HCL (MET). Zero order, first derivative, ratio derivative spectrophotometric methods and flourometric methods have been developed. The zero order spectrophotometric method was used for the determination o...

It is proved that the class of operator equations F(y) = f solvable by a DSM (dynamical systems method) Newton-type method, u̇ = −[F (u) + a(t)I]−1[Fu(t) + a(t)u − f ], u(0) = u0, (∗) is large. Here F : X → X is a continuously Fréchet differentiable operator in a Banach space X , a(t) : [0, ∞) → C is a function, limt→∞ |a(t)| = 0, and there exists a y ∈ X such that F(y) = f . Under weak assumpti...

Predictor-corrector (PC) methods for the numerical solution of stiff ODEs can be extended to include the second derivative of the solution. In this paper, we consider second derivative PC methods with the three-step second derivative Adams-Bashforth as predictor and two-step second derivative Adams-Moulton as corrector which both methods have order six. Implementation of the proposed PC method ...

A new simple and sensitive ratio-spectra first derivative spectrophotometric method was developed for the simultaneous determination of tapentadol hydrochloride (TPH) and paracetamol (PCM) in binary mixtures. The method depends on the use of the first derivative of the ratio-spectra obtained by dividing the absorption spectrum of binary mixture by a standard spectrum of one of the compounds. TP...

the aim of this paper is to study the high order difference scheme for the solution of a fractional partial differential equation (pde) in the electroanalytical chemistry. the space fractional derivative is described in the riemann-liouville sense. in the proposed scheme we discretize the space derivative with a fourth-order compact scheme and use the grunwald- letnikov discretization of the ri...

UNLABELLED BACKGROUND The new combination of moxifloxacin HCl and cefixime trihydrate is approved for the treatment of lower respiratory tract infections in adults. At initial formulation development and screening stage a fast and reliable method for the dissolution and release testing of moxifloxacin and cefixime were highly desirable. The zero order overlaid UV spectra of moxifloxacin and ...

in this article, an analytical approximate solution of nonlinear fractional convection-diffusion with modifiedriemann-liouville derivative was obtained with the help of fractional variational iteration method (fvim). a newapplication of fractional variational iteration method (fvim) was extended to derive analytical solutions in theform of a series for this equation. it is indicated that the so...

Curvature collineations of a spray manifold induced by the Lie symmetries of the underlying spray are studied. The basic observation is that the Jacobi endomorphism and the Berwald curvature are invariant under these symmetries; this implies the invariance of the further curvature data. Our main technical tool is an appropriate Lie derivative operator along the tangent bundle projection. M.S.C....