esterification of chitosan with adipic acid catalyzed by immobilized candida antarctica lipase b was carried out in this study. response surface methodology (rsm) based on a four-factor- five-level small central composite design (sccd) was employed to model and analyze the reaction. a total of 21 experiments representing different combinations of the four reaction parameters including ch...

biodegradation of phenanthrene (phe) was studied in aqueous culture to demonstrate the potential of the mixed culture in degrading high concentration of phe. the experiments were conducted to monitor biodegradation of phenanthrene for duration of 6 days. biodegradation of phe was successfully achieved in low and middle concentration by the isolated mixed culture. a full factorial central compos...

The aim of this study is to explore the capability of subcritical methanol to reduce the acidity of naphthenic acids and to determine reaction kinetics for large-scale reactor design.The experiments were carried out in a 25 mL autoclave reactor (China) at temperatures of 70-120oC, Methanol Partial Pressures (MPPs) of 0.1-1.5 MPa, and reaction times of 0-60 min. The total...

The aim of this study is to explore the capability of subcritical methanol to reduce the acidity of naphthenic acids and to determine reaction kinetics for large-scale reactor design.The experiments were carried out in a 25 mL autoclave reactor (China) at temperatures of 70-120oC, Methanol Partial Pressures (MPPs) of 0.1-1.5 MPa, and reaction times of 0-60 min. The total...

The current study aimed to examine the overall feasibility of the use of copper oxide nanoparticles (CuO-NPs) as a catalyst in ozonation process for the removal of benzene from aqueous solutions under experimental conditions. This experimental study was conducted on a laboratory scale reactor in a semi-batch mode. The effect of critical operating parameters such factors as pH, concentration of ...

polyethylene imide was synthesized from the reaction of high density polyethylene grafted maleic anhydride (pe-g-ma) and 1,4-diaminobutane in boiling xylene. the chemical compositions of the reaction products were examined by fourier transform infrared spectroscopy. different conditions and parameters like the effect of temperature, time, monomer concentration and oxygen on the extent of reacti...