Three new polyfunctional amines were synthesized. Polyimide films containing varying amounts of the amine crosslinking agents were prepared. Their thermomechanical properties were compared with those of control film samples prepared from difunctional amines. The effect of crosslink density on isothermal weight loss, polymer softening, and glass transition temperature is discussed. EFFECTS OF MU...

This paper is devoted to the construction of a computational nonlinear thermomechanical model of large light partition walls made up of cardboard-plasterboard-cardboard (CPC) plates screwed to a metallic frame, and is submitted to mechanical and thermal loadings induced by fire. The computational model, based on experimental analyzes and a probabilistic modeling, is developed for the prediction...

We present a new thermomechanical method and a platform to measure the phase transition temperature at microscale. A thin film metal sensor on a membrane simultaneously measures both temperature and mechanical strain of the sample during heating and cooling cycles. This thermomechanical principle of operation is described in detail. Physical hydrogel samples are prepared as a disc-shaped gels (...

A new treatment of quasistatic (reversible) multiscale processes in heterogeneous materials at nonzero temperature is presented. The system is coarse grained by means of a finite-element mesh. The coarse-grained free-energy functional (of the positions of the nodes of the mesh) appropriate to the thermodynamic-state variables controlled in the relevant process is minimized. Tests of the new pro...

Austenitic stainless steels are extensively used in various applications requiring good corrosion resistance and formability. In the current study, the formation of nano/ ultrafine grained austenitic microstructure in a microalloyed AISI 304L stainless steel was investigated by the advanced thermomechanical process of reversion of strain-induced martensite. For this purpose, samples were subjec...

in this study, the effects cold rolling and annealing parameters during thermomechanical processing of the aisi 201ln stainless steel were investigated. the cast samples were homogenized, hot-rolled and solution-annealed to acquire a suitable microstructure for the subsequent thermomechanical treatment. unidirectional and transverse multi-pass cold rolling at 25, 0 and -15 °c was carried out to...