cadmium sulfide nanoparticles were grown using wet chemical method by dissolving the reactants ofcadmium acetate and sodium sulfide in the presence of thioglycerol (tg) as capping agent in ethanolsolvent. different nanoparticle sizes and size distribution were obtained through varying the molaritiesof thioglycerol. at higher tg concentration, synthesis provides a nearly monodisperse nanoparticl...

Combined low-temperature NMR/UV-vis spectroscopy (UVNMR), where optical and NMR spectra are measured in the NMR spectrometer under the same conditions, has been set up and applied to the study of H-bonded anions A··H··X(-) (AH = 1-(13)C-2-chloro-4-nitrophenol, X(-) = 15 carboxylic acid anions, 5 phenolates, Cl(-), Br(-), I(-), and BF(4)(-)). In this series, H is shifted from A to X, modeling th...

ZnS nanoparticles of different size have been synthesized using a colloidal particles method. ZnS nanoparticles prepared with capping agent (mercaptoethanol) then were characterized using X-ray diffraction (XRD) and UV-Vis spectroscopy. The particle size of the nanoparticles calculated from the XRD patterns has been found in the range 1.85-2.44nm. Absorption spectra have been obtained using UV-...

Spinel zinc manganese oxide (ZnMn2O4) nanorods were successfully prepared using the previously synthesized α-MnO2 nanorods by a hydrothermal method as template. The nanorods were characterized by X-ray diffraction, scanning electron microscopy, transmission electron microscopy, UV-Vis absorption, X-ray photoelectron spectroscopy, surface photovoltage spectroscopy, and Fourier transform infrared...

porphyrins are a ubiquitous large class of naturally occurring macrocyclic compounds with many significant biological representatives comprising heme and chlorophyll. some novel adaptable methods for the synthesis of free-based porphyrins as promising sensitizers for the use in photo-dynamic therapy by the virtue of their known tumor affinity, low dark cytotoxicity, and easy synthesis in good t...

Atomic Absorption Based Techniques. Atomic Fluorescence Spectroscopy. Figure 1.3 Schematic diagram showing the before (left) and after (right) the draw the sample into a nebulizer by the Bernoulli Effect where it is converted. Atomic absorption and emission spectroscopy in the ultraviolet and visible A schematic diagram of a UV-Vis spectrophotometer is shown in Figure.11. Preface Inductively co...

in this research zinc oxide (zno) nano-crystalline powders were prepared by sol-gel method using zinc acetate. the zno nanoparticles were characterized by x-ray diffraction (xrd), scanning electron microscopy (sem), ultraviolet-visible (uv-vis), fourier transform infra-red (ft-ir) and energy dispersive x-ray (edx) spectroscopy. the structure of nanoparticles was studied using xrd pattern. the c...

UV–VIS spectroscopy is applied to study the structural and especially morphological particularities of silver nanoclusters-phosphate glass composites from the dispersed phase perspective. The electronic absorption measurements performed on several types of phosphate glasses with different Ag2O content indicate the existence of both silver nanoparticles of various dimensions and shapes, and Ag i...

Nanocrystals of ZnO were prepared by microwave irradiation using Zn (II) acetate and triethanol amin (TEA) as the starting materials and water as solvent. The nanocrystals of ZnO with hexagonal (Wurtzite) structure were characterized by X-ray powder diffraction (XRD), transmission electron microscopy (TEM), scanning electron microscopy (SEM), UV-Vis absorption and FTIR Spectroscopy techniques.