This paper discusses the sorbent properties of magnetic activated carbons and biochars produced by wet impregnation with iron oxides. The sorbents had magnetic susceptibilities consistent with theoretical predictions for carbon-magnetite composites. The high BET surface areas of the activated carbons were preserved in the synthesis, and enhanced for one low surface area biochar by dissolving ca...

Supercritical impregnation is an attractive “clean” alternative to conventional soaking into liquid process, using generally organic solvents. Impregnation process can be used for the development of controlled delivery systems that can be applied in pharmaceutical and medical fields. This work focuses on the preparation of controlled drug delivery systems for ophthalmic applications through sup...

A series of Mn-Co/TiO2 catalysts were prepared by wet impregnation method and evaluated for the oxidation of NO to NO2. The effects of Co amounts and calcination temperature on NO oxidation were investigated in detail. The catalytic oxidation ability in the temperature range of 403–473 K was obviously improved by doping cobalt into Mn/TiO2. These samples were characterized by nitrogen adsorptio...

Self-organized TiO 2 nanotubes (TNTs) with average inner diameter of 109 nm, wall thickness of 15 nm, and tube length of 7– 10 μm were loaded with nickel oxide (NiO) nanoparticles via incipient wet impregnation method. The molar concentration of Ni(NO 3 ) 2 ⋅6H 2 O aqueous solution varied in a range of 0.5M–2.5M. The samples were characterized for crystalline phase, morphology, topography, chem...

The effect of adding oxide promoters, at monolayer coverages, to Pd/ceria catalysts was studied for the watergas-shift reaction in 25 torr each of H2O and CO under differential conditions. Oxides of Fe, Tb, Gd, Y, Sn, Sm, Pr, Eu, Bi, Cr, V, Pb, and Mo were added to ceria by wet impregnation of aqueous salts and calcined to 873 K prior to addition of 1 wt% Pd. While most of the oxides had a negl...

Traditional nanosized photocatalysts usually have high photocatalytic activity but can not be efficiently recycled. Film-shaped photocatalysts on the substrates can be easily recycled, but they have low surface area and/or high production cost. To solve these problems, we report on the design and preparation of efficient and easily recyclable macroscale photocatalysts with nanostructure by usin...

Ag-Cu supported on activated carbon (Ag-Cu/C) catalysts with different compositions of Ag and Cu (total loading of Ag + Cu =1 weight %) were prepared by wet impregnation technique. These catalysts were characterized by BET surface area XRD, TPR, TEM and XPS. The catalytic activity of these catalysts was tested for control of microorganism in drinking water by nutrient agar coating method. Catal...

We have developed a new experimental platform for in situ scanning transmission electron microscope (STEM) energy dispersive X-ray spectroscopy (EDS) which allows real time, nanoscale, elemental and structural changes to be studied at elevated temperature (up to 1000 °C) and pressure (up to 1 atm). Here we demonstrate the first application of this approach to understand complex structural chang...

Multiwall carbon nanotubes (CNTs) and iron oxide impregnated carbon nanotubes (CNTs-iron oxide) were investigated for the adsorption of hazardous toluene and paraxylene (p-xylene) from aqueous solution. Pure CNTs were impregnated with iron oxides nanoparticles using wet impregnation technique. Various characterization techniques including thermogravimetric analysis, scanning electron microscopy...