A non-invasive XRD/XRF instrument for study of works of art has been developed jointly by the Getty Conservation Institute and inXitu Inc. (California). Many aspects of the instrument are based on technologies initially developed for NASA’s planetary XRD/XRF instrument CheMin and used in inXitu’s portable transmission XRD/XRF instrument (Terra). A new geometry was designed based on a reflection...

Since zeolites are notoriously difficult to prepare as large single crystals, structure determination usually relies on powder X-ray diffraction (XRD). However, structure solution (i.e., deriving an initial structural model) directly from powder XRD data is often very difficult due to the diffraction phase problem and the high degree of overlap between the individual reflections, particularly f...

Data from X-ray powder diffraction (XRD) were subjected to a partial least-squares regression analysis (PLS) to build a calibration model for predicting the polymorphic content of carbamazepine (CBZ). The effectiveness of the PLS method in the construction of calibration models was analyzed by a scientific approach based on a regulation vector. CBZ forms I and III were characterized by differen...

This work presents the results for identification of chemical phases obtained by several laboratories as a part of an international nuclear forensic round-robin exercise. In this work powder X-ray diffraction (p-XRD) is regarded as the reference technique. Neutron diffraction produced a superior high-angle diffraction pattern relative to p-XRD. Requiring only small amounts of sample, µ-Raman sp...

A technique based on x-ray diffraction (XRD) is introduced to understand the variation of the grain-to-grain ordering in FePt recording media. We classify the possible ways that the grains may be ordered into three types: homogeneous ordering, inhomogeneous ordering, and bipolar ordering. We study the possible impact of each type of ordering on the XRD spectra in terms of the relative angular p...