A novel class of aryl vinyl ethers 3 and diethyl 3-cyano-3-alkylprop-1-en-2-ylphosphonates 4 has been prepared, respectively, from coupling reaction of diethyl 1-(bromomethyl)-2-cyanovinylphosphonate 2 with phenols and Gilman reagents.

Synthesis and characterization of 6-(hydroxymethyl)-14, 16-dimethyl-13, 14, 16, 17-tetrahydro-6H-13, 17-epiminodibenzo [e, l] [1, 4] dioxacyclotridecin-15 (7H)-oneABSTRACTNew 6-(hydroxymethyl)-14, 16-dimethyl-13, 14, 16, 17-tetrahydro-6H-13, 17-epiminodibenzo [e, l] [1, 4] dioxacyclotridecin-15 (7H)-one (2a) was synthesized in good yield by the Petrenko–Kritchenko reaction of 2, 2'-((3-hydroxyp...

Here, we investigated the physicochemical and storage characteristics of Tteokgalbi using n-3 fatty acid-enriched pork (n-6/n-3 ratio: 3.220) explored effects treatment with watermelon radish powder (W; 0–4%). groups were prepared 0% W (control (CON)), 1% (W1), 2% (W2), 4% (W3), or 0.05% ascorbic acid as a reference (REF) treatment. addition to increased moisture ash contents water-holding capa...

General information. All manipulations were performed in a N2 filled drybox or using standard Schlenk techniques. Allyl benzene, methyl vinyl ketone, pchlorostyrene, methyl methacrylate, diethyl diallylmalonate (3), and 1,6-heptadien-4ol (6) were purchased from Aldrich and used without further purification. cis-4Cyclopentene-1,3-diol and (+)-citronellal were purchased from Fluka and used withou...

Constructing ternary structure is one of the most effective design strategies to break efficiency ceiling traditional binary organic solar cells (OSCs). Here, a new Y-series non-fullerene acceptor (Y-T) featuring 1,3-diethyl-2-thiobarbituric acid (DTBA) end groups developed as third component for classical PM6:Y6 system. The champion power conversion OSCs increased from 15.64% 17.37% via incorp...