In this research, we synthesized oxazine and thiazine derivatives (3-6). These of chacone compounds (1 2) that from 4- hydroxyacetophenone aldehyde such as, 4-bromobenzaldehyde chlorobenzaldehyde. chalcone (1-2) reacted with urea to produce as 4-[4-amino-6-(4-subsutitedphenyl)-2H-1,3-oxazin-2-yl] phenol (3 4) thiourea 4-[4-amino-6-(4-subsutitedphenyl)-2H-1,3-thiazin-2-yl] (5 6). were characteri...

This work is concerned with the preparation of a number organic ammonium formate salts (or ionic liquids; ILs) throughout reaction between formic acid and some aliphatic aromatic amines including ammonia. Five were formed, them in form solid others as liquids (ILs) at room temperature. The yields prepared ranged from (21%) to (79%). However, attempts towards other fifteen not successful. result...

A series of N-substituted-2,4-thiazolidinedione derivatives (TZDs) were prepared via N-alkylation of 2,4-TZD at position 3 using substituted benzyl halides. Synthesized N-substituted-2,4-TZD was then substituted at position 5 with substituted aromatic aldehyde according to Knoevenagel condensation method. Structures of the compounds were elucidated using various spectral techniques viz. IR, 1HN...

A series of different N-4-piperazinyl derivatives of norfloxacin was synthesized and screened for their antibacterial, antifungal and cytotoxic activities to monitor the variation in therapeutic effects of parent molecule. Result revealed that some of the tested compounds showed comparable or better activity than norfloxacin against Gram positive bacteria and Gram negative bacteria. The structu...

a series of transition metal complexes with two thiosemicarbazide schiff bases, 1-(4-dimethylaminobenzyl- idene)thiosemicarbazide (abtsc) and 1-(2-pyridincarboxyl-idene) thiosemicarbazide (tcts) were synthesized with co(ii), ni(ii), zn(ii), cd(ii) and ag(i) salts (chloride and acetate). these complexes were characterized by different methods including proton nuclear magnetic resonance (1hnmr), ...

heavy alkylated benzene (hab), which is a by-product in linear alkylbenzene (lab) production by uop process, is separated by distillation from lab and consists of a range of components such as polyalkylbenzenes, diphenylalkanes, alkyl tetralins, and alkylindans. the products of sulfonation of hab or its distillation cuts are of wide industrial applications such as emulsifiers, dispersants in lu...

In this work, magnetic mesoporous silica-alumina composites (MSA) containing three metal oxides(MSA/MO) with different molar ratio of Si to Al (0.5, 1 and 2) were synthesized. The efficiency prepared catalysts was compared modified natural zeolite (ferrierite) in the multicomponent synthesis indeno[1,2-b]indole-9,10-diones. Immobilization ZnO, CuO NiO on increased their Lewis acidic sites impro...

Abstract Diphenylamine (DPA), formyl chloride, and sodium hydride (NaH) as raw materials synthesize methyldiphenylurea stabilizer by alkylation reaction. The physical chemical properties of were characterized nuclear magnetic resonance hydrogen spectrum (1HNMR), X-ray energy (EDS), Fourier transforms infrared spectroscopy (FT-IR) differential thermal analysis (DTA). Thermal Decomposition Experi...