The thermal calcination of borax pentahydrate was investigated for both dehydration and decomposition steps at temperatures between 392 and 573 K in a controlled fluidized bed drier. The best kinetic parameters (reaction rate constants, reaction order and equilibrium values) of both steps were determined by the genetic algorithm (GA) method for each calcination temperature in respect of relativ...

Mixed copper-cerium oxides were prepared by two methods leading to different wpper species in the as-prepared material. At the catalyst operating temperature (300400°C) and above, the same copper species was present irrespective of the prepration technique. A solid solution having the same fluorite structure as that of pure CeQ was formed and remained stable after calcination to 100O0C. At temp...

Abstract— The effect of calcination temperature on the morphology of plating sludge generated from waste water treatment plant was studied. This waste was hazardous waste due to high toxic metal content [1]. It must be recovered, reuse or recycled before the process but its properties should determined in order to decide recovery method [2]. Previous researches were shown that this kind of wast...

The composites graphite/ZnO were prepared using calcination method. Zinc chloride (ZnCl2) and sodium carbonate (Na2CO3) were used for synthesis of zinc oxide (ZnO), whereas micromilled and natural graphite were used as the matrix for ZnO nanoparticles growing. During the reaction of ZnCl2 with saturated aqueous solution of Na2CO3 new compound Na2Zn3(CO3)4•(H2O)3 originates. During the calcinati...

ZnFe2O4 mixed spinel ferrite nanoparticles obtained through a citrate-nitrate combustion method. Ignited products calcined at different temperatures in 600-900ºC range and effect of calcination treatment temperature investigated. Final Products characterized by X-ray Diffraction (XRD), Fourier-Transform Infrared spectroscopy (FTIR), and Field Emission Scanning Electron Microscopy (FESEM). The a...

The NbSe2 nanoplates with novel hexagonal morphology have been obtained via solid-state assembly of NbSe2 ultrathin nanosheets, which were prepared by a simple calcination process using micro-sized Nb and Se powders as the precursors. The influence of high-temperature annealing upon morphology of single-crystal NbSe2 was investigated. On the basis of experimental results of different temperatur...

Synthetic fluorspar can be produced from waste calcium fluoride slurry settled on dumpsites located near Cracow centre. Synthetic fluorspar exchanges natural raw material used in the metallurgical industry. To obtain grained synthetic fluorspar, calcium fluoride slurry should be calcinated in rotary kilns at temperatures of 900-1100K. Grain size and compression strength strongly depends on calc...

In this work, hydrochloric acid is used to remove iron impurities in the bauxite ore contained in the diasporite mineral located in the Sari region. The bauxite ore was calcined at different temperatures and times, and then dissolved in a hydrochloric acid solution. After determining the optimum calcination conditions in 1 h at 900 °C, the response surface methodology (RSM) with four factors in...

The presence of elevated concentration of arsenic in water sources is considered to be health hazard globally. Calcination process is known to change the surface efficacy of the adsorbent. In current study, five adsorbent composites: uncalcined and calcined Fe3O4-HBC prepared at different temperatures (400°C and 1000°C) and environment (air and nitrogen) were investigated for the adsorptive rem...

Effects of calcination temperatures varying from 400 to 1000°C on structural and magnetic properties of nanocomposites formed by Co-ferrite dispersed in the sol-gel silica matrix using tetrakis(2-hydroxyethyl) orthosilicate (THEOS) as water-soluble silica precursor have been investigated. Studies carried out using XRD, FT-IR, TEM, STA (TG-DTG-DTA) and VSM techniques. Results indicated that magn...