نتایج جستجو برای: electrospray
تعداد نتایج: 8566 فیلتر نتایج به سال:
This review addresses the determination of the internal energy of ions produced by electrospray ionization (ESI) sources, and the influence of the internal energy on analyte fragmentation. A control of the analyte internal energy is crucial for several applications of electrospray mass spectrometry, like structural studies, construction of reproducible and exportable spectral libraries, analysi...
OBJECTIVE Early identification of causative microorganism(s) in patients with severe infection is crucial to optimize antimicrobial use and patient survival. However, current culture-based pathogen identification is slow and unreliable such that broad-spectrum antibiotics are often used to insure coverage of all potential organisms, carrying risks of overtreatment, toxicity, and selection of mu...
Electrospray is the technique to soft-ionize liquids by applying a high electric potential to a liquid meniscus. The liquid meniscus is deformed into a cone [1], and charged species are emitted from its apex. The emission can be solvated ions, charged droplets, or a mix of the two. This low-divergence charged species source can be used in diverse applications such as mass spectrometry, propulsi...
T detection and identification of molecules within complex biological matrixes (i.e., plant tissue) requires homogenization, filtration, and liquid extraction of the sample to prepare for analysis using techniques such as gas chromatography/mass spectrometry (GC/MS), liquid chromatography-mass spectrometry (LC-MS), capillary electrophoresis-mass spectrometry (CE-MS), and LC-NMR. Direct analysis...
Most hyphenated analytical approaches that rely on liquid chromatography-MS require relatively long separation times, produce incomplete resolution of oligosaccharide mixtures, use eluents that are incompatible with electrospray ionization, or require oligosaccharide derivatization. Here we demonstrate the analysis of heparin oligosaccharides, including disaccharides, ultralow molecular weight ...
A sensitive, fast, low-cost and simple determination method was developed for the of nicotine in smokeless tobacco (Maras powder) using liquid chromatography-electrospray ionization tandem mass spectrometry. With method, amount Maras powder ashy determined confirmed. Chromatographic separation performed on a Hypersil Gold (2.1 mmx200 mm, 1.9 um) at 30 ◦C with gradient 0.2% acetic acid water ace...
Multitrack electrospray chips (MTEC) were fabricated by UV-photoablation of polyethylene terephthalate (PET) substrates. They are composed of an array of up to six microchannels that are successively used as electrospray ionization (ESI) emitters for mass spectrometry (MS). There is no requirement for alignment of the different spraying microchannels with the mass spectrometer orifice. The MTEC...
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