This procedure has developed the use of TiO2 nanoparticles as an environmentally friendly and highly efficient heterogenous nanocatalyst for the eco-safe, facile and one-pot three-component Biginelli synthesis of biologically active corresponding 3,4-dihydropyrimidin-2-(1H)-one/thione derivatives under solvent-free conditions. This eco-friendly protocol provi...

In the present work, we report the synthesis of binary nano metal oxides such as Zinc /Copper Oxide via novel dry synthetic methods such as thermal decomposition of oxalate precursor. The synthesis route involves facile solid-phase mechanochemical activation of a physical mixture of simple copper/zinc salts and oxalic acid, followed by calcination of the as-ground oxalate precursors at 450◦C. X...

an improved, simple, and facile synthesis of 3,4-dihydropyrimidin-2(1h)-ones by employing three-component, one-pot condensation reaction of β-keto ester, aromatic aldehydes, and urea or n-methylurea using lacl3/clch2cooh as an inexpensive and green chemistry catalyst system under solvent-free conditions described. compared with the classicalbiginelli reaction conditions, this method has the adv...

a facile one step synthesis of anilino alky1-n-substituted phthalimide i is reported. the following compounds belonging to this series were made: 1. (anilino-n-ethyl) phthalimide 8 2. (3,4, 5-trimethoxy anilino-n-ethyl) phthalimide 6 3. (3,4, 5-trimethoxy anilino-n-propyl) phthalimide 7 4. n-(ethyl phthalirnido-p-amino benzoyl) glutamic acid diethyl ester 10 5. n-(propyl phthalimido-p-amino ben...

CD44v6 peptide functionalized nanoparticles are fabricated in a facile and controllable way to selectively bind to CD44v6 positive tumor cells with highly efficient anticancer and antimetastatic properties. The reported modular synthesis and facile preparation makes this system highly potent for developing novel multifunctional nanocarriers for therapeutic and/or diagnostic anticancer applicati...

A one-pot synthesis of (S)-(-)-propranolol is reported. Zn(NO3)2/(+)-tartaric acid catalyzed enantioselective synthesis of (S)-(-)-propranolol via kinetic resolution of key intermediate ?-naphthyl glycidyl ether with high optical and chemical yield.

A rapid and facile synthesis of cubic MCM-48 mesoporous material based on the modification of Stöber synthesis in as little time as 30 minutes at room temperature is reported in this communication.

Cu2SnS3 (CTS) nanorods were synthesized with a controllable aspect ratio via a facile phosphine-free colloidal synthesis. This synthesis can be readily extended to obtain Cu2ZnSnS4 (CZTS) nanorods with tunable Zn content.

a facile mechanochemical-based method for synthesis of copper oxide (cuo) nanoparticles is here by introduced. for this purpose, copper hydroxide powder was synthesized through a facile solution method (cuso4 + 2 na(oh) → cu(oh)2 + na2so4) after which milling of as-prepared cu(oh)2 precursor and nacl resulted in the mechanochemical dehydration of cu(oh)2 and dispersion of cuo nanoparticles into...

cuals2  chalcopyrite  nanocrystalline  are  synthesized  with  facile method.  the  heat  arrested  solvothermal  method  for  synthesize nanocrystalline  were  investigated.  the  time  duration  of  synthesis, temperature of solution and metal salts to solvent molar ratio can be parameters  that we are  studied. the nanoparticles were  synthesized with cucl, alcl3 and  thiourea (sc(nh2)2) as ...