نتایج جستجو برای: gas chromatography flame ionization detection
تعداد نتایج: 908313 فیلتر نتایج به سال:
A solid-phase microextraction (SPME) sampling method is developed to evaluate indoor exposure to benzene, toluene, ethylbenzene, xylene, and styrene with gas chromatography and flame ionization detection for quantitative analysis. An SPME holder with a 100-pm polydimethylsiloxane (PDMS) and 65-pm PDMS-divinylbenzene fiber coating is tested in different air relative humidity conditions. The meth...
A validated method for the determination of validol in tablet dosage forms using gas chromatography with flame-ionization detection and n-octanol as the internal standard is developed. Validol represents a 25-30% solution of menthol in the menthyl ester of isovaleric acid. The separation of both compounds was achieved on a HP-FFAP (nitroterephthalic acid modified polyethylene glycol) fused sili...
a simple and rapid microextraction procedure based on dispersive liquid-liquid microextraction (dllme) coupled with gas chromatography-flame ionization detection (gc-fid) was developed for the extraction and analysis of 2-phenylethanol in rose water sample. in the proposed approach, carbon tetrachloride and ethanol were used as extraction and dispersive solvents, respectively. some important pa...
Because cholesterol and its oxide products (COPs) are used as standards during analysis, their stability and autoxidation were assessed under typical storage conditions. Individual toluene solutions of cholesterol; cholesterol5β, 6β-epoxide; cholesta-3,5-dien-7-one; and 5α-cholestane were prepared and aliquots were stored at 23 ± 2°C, 4°C, and -20°C for 7 days. Samples were removed from storage...
Oleic acid is a common pharmaceutical excipient that has been widely used in various dosage forms. Gas chromatography (GC) has often been used as the quantitation method for fatty acids normally requiring a derivatization step. The aim of this study was to develop a simple, robust, and derivatization-free GC method that is suitable for routine analysis of all the major components in oleic acid ...
Chemical composition of the essential oil obtained from the aerial parts of Scrophularia amplexicaulis Benth. was analyzed, for the first time, by the gas chromatography/mass spectrometry (GC-MS) and gas chromatography/flame ionization detection (GC-FID). A total yield of 3 mg of essential oil per100 g of plant dry mass was obtained, and 27 compounds were identified, representing 97.7% of total...
The data presented in this article describe the fatty acid composition of chow, liver tissue and isolated liver mitochondria from mice fed for 6-24 weeks with a high caloric western diet (WD) in comparison to control diet (normal diet, ND). The fatty acid composition was measured via gas chromatography flame ionization detection (GC-FID). Moreover, WD-induced mitochondrial protein changes are p...
A preparative gas chromatography (pGC) method was developed for the separation of isomers (cis- and trans-asarone) from essential oil of Acorus tatarinowii. The oil was primarily fractionated by silica gel chromatography using different ratios of petroleum ether and ethyl acetate as gradient elution solvents. And then the fraction that contains mixture of the isomers was further separated by pG...
A rapid, sensitive and selective gas chromatographic method with flame ionization detection was developed for the determination of paraldehyde in small blood samples taken from children. Whole blood samples (300 microl) collected in a 3 ml Wheaton glass sample vial were spiked with acetone (internal standard: 15 ng) followed by addition of concentrated hydrochloric acid. The mixture was heated ...
Submit Manuscript | http://medcraveonline.com Abbreviations: GLPs: Gracilaria Lemaneiformis Polysaccharides; FTIR: Fourier Transform Infrared Spectroscopy; GC: Gas Chromatography; HPGPC: High Performance Gel Permeation Chromatography; NK: Natural Killer; IL-2: Interleukin-2; IFN-γ: Interferon-γ; TNF-α: Tumor Necrosis Factor-α; BRM: Biological Response Modifier; ConA: Concanavalin A; LPS: Lipo P...
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