In this study, the grain boundary character and texture of 50% and 90% cold-rolled FePd alloy was investigated during recrystallization at 700 °C. Electron backscatter diffraction (EBSD) measurements were performed on the rolling direction to normal direction section. Kernel average misorientation (KAM) calculated from EBSD measurements was employed to determine the recrystallization fraction. ...

Steinernema feltiae is a moderately freezing tolerant nematode, that can withstand intracellular ice formation. We investigated recrystallization inhibition, thermal hysteresis and ice nucleation activities in the infective juveniles of S. feltiae. Both the splat cooling assay and optical recrystallometry indicate the presence of ice active substances that inhibit recrystallization in the nemat...

Quantitative analysis of boundary migration during recrystallization is a key task to understand the recrystallization process and to improve recrystallization models. In the last 2530 years, quantification of boundary migration has mostly been conducted in term of average growth rates in many materials. This type of analysis has largely been based on the assumption that all or groups of recrys...

Total scattering pair distribution function (TSPDF) analysis of synchrotron X-ray diffraction data has been used to study the structural characteristics of amorphous lactose and its subsequent recrystallization on aging. This shows that the recrystallization kinetics vary substantially between spray dried, lyophilized, and melt quenched samples aged at 40 °C/75% relative humidity (RH), although...

The development of recrystallization textures in two low carbon steels used for deep drawing has been investigated through measurements of global textures (by X-Ray diffraction) and local orientations (by EBSD, Electron Back Scattering Diffraction). The global measurements allow a quantitative description of the recrystallization textures whereas the local measurements allow to identify some of...

In this study, the grain boundary evolution of equiatomic CoCrFeMnNi, CoCrFeNi, and FeCoNi alloys after one-step recrystallization were investigated. The special boundary fraction and twin density of these alloys were evaluated by electron backscatter diffraction analysis. Among the three alloys tested, FeCoNi exhibited the highest special boundary fraction and twin density after one-step recry...

The evolution of texture as a function of recrystallization has been characterized for hot-rolled AA1050. Samples prepared from a hot rolled sheet were annealed isothermally for sufficient time to allow complete recrystallization. The spatial orientation variation within the deformed microstructure of nucleation, growth and orientations of recrystallized grains is examined. The microstructural ...

Recrystallization in copper deformed by dynamic plastic deformation was investigated using electron backscatter diffraction. The recrystallized grains show a broad size distribution. The kinetics of grains of different sizes is observed to be different: In the beginning of recrystallization, the area fraction of small recrystallized grains increases rapidly. At later stages of recrystallization...

Solid-state properties of piroxicam benzoate, an ester prodrug of piroxicam, were investigated. Samples were prepared by recrystallization from various organic solvents (toluene, ethanol, methanol, ethyl acetate and acetone). Recrystallized samples were characterized by means of FTIR, DSC, TGA, SEM and XRPD. DSC, TGA and XRPD methods confirmed that piroxicam benzoate crystallized in two pseudop...

The interaction of calcite with trivalent europium under recrystallization conditions was studied on the molecular level using site-selective time-resolved laser fluorescence spectroscopy (TRLFS). We conducted batch studies with a reaction time from seven days up to three years with three calcite powders, which differed in their specific surface area, recrystallization rates and impurities cont...