cu2o nanoparticles were synthesized by thermal treatment in liquid paraffin without any inert gas protection using nano structures of schiff base copper (ii) complex (1) as precursor. liquid paraffin was used as solvent and reductant. span 80 was applied to control the morphology of cuprous oxide nanoparticles. the nano structure of the complex was characterized by x-ray diffraction measurement...

SiO2 coated γ-Fe2O3 nanocomposite powder has been successfully synthesized by chemical vapor condensation process and its feasibility on hyperthermic application was investigated in this study. The power loss of SiO2 coated γ-Fe2O3 nanocomposite powder which means the magnetic heating effect under alternative magnetic field was much higher than the single phase γ-Fe2O3 nano powder due to the ve...

Abstract This study examined the influence of crystallinity added nano-alumina on sulfate resistance ordinary Portland cement (OPC) paste. Two crystalline types nano-aluminas (α-and γ-phase) were incorporated in pastes, which exposed to solution. In results, both paste samples having α- and γ-phase aluminas had accelerated compressive strength loss increased length expansion compared sample wit...

chemical vapor deposition was employed to synthesize carbon nanotubes with ni-loaded mcm-41 and mcm-48 as catalysts and acetylene as precursor at 750°c. mesoporous ni mcm-41 and ni mcm-48 molecular sieves were synthesized by a hydrothermal method and were characterized by xrd and n2 adsorption isotherm. the catalytically synthesized carbon materials were characterized with raman spectroscopy, n...

zno thin films were deposited on si(400) substrates by e-beam evaporation technique, and then post-annealed at different annealing temperatures (200-800°c). dependence of the crystallographic structure, nano-strain, chemical composition and surface physical morphology of these layers on annealing temperature were studied. the crystallographic structure of films was studied using x-ray diffracti...

In the present study, the gamma alumina (γ-Al2O3) nano powders have been prepared with addition of 1%mol Co using an aqueous sol-gel method at lower temperature than the pure gamma alumina. The synthesis process accomplished by partial hydrolysis of the aqueous solution of metallic ions Al3+ and Co2+, with ammonia. The Al(NO3)3.9H2O and Co(NO3)2.6H2O salts were used as cations sources. The obta...

Transparent polycrystalline ceramics exhibit improved mechanical and optical properties. However, synthesizing transparent without additives is nontrivial. Herein, we report the synthesis of two (β-Si3N4 γ-Si3N4) under high pressure temperature from a pure Si3N4 precursor with nano-/micro-dual grain sizes. Synthesized β-Si3N4 exhibited significantly enhanced Vickers hardness reaching 24.2 GPa (...

mammalian ∆-(1)-pyrroline-5-carboxylate synthase (p5cs) enzyme catalyzes the coupled phosphorylation and reduction-conversion of glutamate to ∆-(1)-pyrroline-5-carboxylate (p5c), a critical step in the proline, ornithine, citrulline and arginine biosynthesis. in plants and mammals, p5cs consists of two separate enzymatic domains: n-terminal γ-glutamyl kinase (γ-gk) and c-terminal γ-glutamyl pho...

to investigate non-bonded interaction of phenanthrene and bn nanostructure, geometric structure of phenanthrene and b12n12 nano-ring with b3lyp method and 6-31g* basis set are optimized by using ab initio gaussian quantum chemical package. the main purpose of this study was to evaluate changes of electronic properties of aromatic compound in presences nano ring field. therefore reactivity and s...

Abstract The mechanical properties of ceramic granular γ-alumina, including resistance and stability, are examined using Nano indentation scratch tests. In so doing, surface morphology, kind material used, topography, roughness the evaluated a scanning electron microscope, energy-dispersive X-ray spectroscopy atomic force microscopy. To achieve these objectives, initial step involves synthesis ...