A new Vis spectrophotometric method was developed for the assay of bisoprolol in pharmaceutical preparations using bromocresol green in hydrochloric acidic medium. The reaction product showed a maximum absorbance at 402 nm proportional with the concentration of bisoprolol. The optimum conditions for the reaction were established. The developed method was validated. The method showed a good line...

two-layer metallic sheets have wide applications in aerospace, marine, automotive and domestic industries due to their superlative characteristics. in this paper, the formability of two-layer sheet is investigated through analytical, experimental and numerical approaches. an analytical model is developed based on marciniak-kuczynski method associated hill’s non-quadratic yield criterion. formin...

A catalytic-kinetic method for the determination of selenium is proposed. Alizarin navy blue is reduced by sodium sulfide to from a colorless product. The reaction is accelerated by trace amounts of Se (IV), and can be followed by measuring the decrease in absorbance of the dye at 620nm and 30 °C by the fixed time method. Selenium can be determined in the range of 0.004 — 0.12 1.1g.m1-1 . ...

nowadays statistical control process plays an important role in quality control of products. so wide variety of methods are utilized to do so. but since the most percentage of available information in the discrete control charts are verbal terms, fuzzy and vague ,in most cases it is difficult for us to refine them into the quantitative data. thus in this article we are to change these verbal da...

A new catalytic kinetic spectrophotometric procedure for determination of trace quantities of zirconium was proposed. Janus Green was oxidized by potassium bromate and zirconium catalyst which then converted to a colorless product in acidic media. Reaction rate was monitored spectrophotometrically at 606 nm. It relies on the linear relationship between the absorbance difference (ΔAt) and Zr(IV)...

In this study, ultrasonic-assisted matrix solid-phase dispersion (UA-MSPD) as a new sample preparation method for natural product analysis was developed. Influential parameters of the UA-MSPD method was optimized using oleuropein content of olive leaves as a model analyte. Main parameters of the proposed technique such as ultrasonic time, amplitude and pulse, sorbent material, the ratio of samp...

2-amino-4-chlorophenol (ACP) is a synthetic precursor of the skeletal muscle relaxant; chlorzoxazone. A rapid simple colorimetric method was proposed for the determination of 2amino-4-chlorophenol as a potential impurity in chlorzoxazone bulk powder via its reaction with 4-aminoantipyrine in presence of alkaline oxidizing agent (K3[Fe(CN)6] / NH3) and measuring the produced red color at 520 nm....