نتایج جستجو برای: ray diffraction and micro

تعداد نتایج: 16903940  

Journal: :iranian endodontic journal 0
hengameh akhavan pooneh mohebbi amir firouzi mehdi noroozi

introduction: the aim of this study was to compare the chemical compounds of white proroot mineral trioxide aggregate (wmta) hydrated at different ph environments. methods and materials: mixed samples of wmta were kept in acidic (ph=5.4), neutral (ph=7.4) and alkaline (ph=9.4) environments for 48 h. then, x-ray diffraction (xrd) analysis was performed for both hydrated and powder forms of wmta....

Journal: :international journal of nano dimension 0
a. bagheri gh. department of chemistry, center tehran branch, islamic azad university, tehran, iran. z. mirjani kahaki department of chemistry, center tehran branch, islamic azad university, tehran, iran.

oxide nanoparticles can exhibit unique physical and chemical properties due to their limited size and a high density of corner or edge surface sites. in this study, mgo nanoparticle was synthesized using mg(ch3coo)2 and hexamethylenetetramine as starting materials. the structure and optical properties of these particles are investigated by using x-ray diffraction (xrd), scanning electron micros...

Journal: :international journal of nano dimension 0
a. jegan. department of chemistry, sona college of technology, salem, india. a. ramasubbu department of chemistry, government arts college (autonomous), coimbatore, india. s. saravanan department of chemistry, sona college of technology, salem, india. s. vasanthkumar department of chemistry and nanotechnology, karunya university, coimbatore, india.

the magnetite (fe3o4) – agar nanocomposite was prepared by co-precipitation of fe (iii) and fe (ii) ions for the first time. the obtained samples were characterized by x-ray diffraction, fourier-transform infrared spectroscopy, scanning electron microscopy and transmission electron microscopy. ft-ir results confirm the formation of fe3o4 nanoparticles in agar matrix. the xrd results revealed th...

2004
Hongqiang Chen Lawrence Yao Jeffrey W. Kysar I. Cev Noyan Youneng Wang

X-ray micro-diffraction profiles using a synchrotron light source were analyzed via Fourier transformation for single crystal Aluminum and Copper samples subjected to micro-scale laser shock peening. Specifically, the asymmetric and broadened diffraction profiles registered across the shock peen region were observed and analyzed by classic Warren and Averbach (W–A) method [Warren, B.E., Averbac...

2017
A. Abboud C. Kirchlechner J. Keckes T. Conka Nurdan S. Send J. S. Micha O. Ulrich R. Hartmann L. Strüder U. Pietsch

The full strain and stress tensor determination in a triaxially stressed single crystal using X-ray diffraction requires a series of lattice spacing measurements at different crystal orientations. This can be achieved using a tunable X-ray source. This article reports on a novel experimental procedure for single-shot full strain tensor determination using polychromatic synchrotron radiation wit...

Journal: :J. Information Science 1988
D. Alasdair Kemp

Research activity: Materials science of magnetic and ferroelectric oxides, semiconductor nanostructures, optoelectronic device design, and characterization of monolithically-integrated GaNand InP-based optoelectronic devices. Primary research interest is in the field of far-IR Ellipsometry, Transmission, and Raman Spectroscopy, Nanoscale High-Angular Resolution X-ray Diffraction, X-ray Standing...

پایان نامه :وزارت علوم، تحقیقات و فناوری - دانشگاه شیراز 1357

این کوپلیمرها از هیدرولیز شاخه جانبی متیل استر، پلی متیل - گلوتامات با کنترل کردن هیدرولیز بدست میایند. مطالعه دستگاه اسپکتروسکپی ir بما نشان میدهد که تقریبا" تمام این کوپلیمرها بصورت a-helix میباشند اگرچه مقدار جزئی از فرم b در آنها دیده میشود. مطالعه x-ray diffraction نشان میدهند که دزیر 50 درصد هیدرولیز، هر دو حالت کریستالی و بی شکل در غشاهای کوپلیمری اولیه دیده میشود، ولی بالاتر از50 درصد ه...

Journal: :Acta Crystallographica Section A Foundations of Crystallography 2010

2015
Thomas D. Murray Artem Y. Lyubimov Craig M. Ogata Huy Vo Monarin Uervirojnangkoorn Axel T. Brunger James M. Berger

Microcrystals present a significant impediment to the determination of macromolecular structures by X-ray diffraction methods. Although microfocus synchrotron beamlines and X-ray free-electron lasers (XFELs) can enable the collection of interpretable diffraction data from microcrystals, there is a need for efficient methods of harvesting small volumes (<2 µl) of microcrystals grown under common...

Journal: :The Review of scientific instruments 2014
D Fan L Lu B Li M L Qi J C E F Zhao T Sun K Fezzaa W Chen S N Luo

Real time, in situ, multiframe, diffraction, and imaging measurements on bulk samples under high and ultrahigh strain-rate loading are highly desirable for micro- and mesoscale sciences. We present an experimental demonstration of multiframe transient x-ray diffraction (TXD) along with simultaneous imaging under high strain-rate loading at the Advanced Photon Source beamline 32ID. The feasibili...

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