introduction: the aim of this study was to compare the chemical compounds of white proroot mineral trioxide aggregate (wmta) hydrated at different ph environments. methods and materials: mixed samples of wmta were kept in acidic (ph=5.4), neutral (ph=7.4) and alkaline (ph=9.4) environments for 48 h. then, x-ray diffraction (xrd) analysis was performed for both hydrated and powder forms of wmta....

oxide nanoparticles can exhibit unique physical and chemical properties due to their limited size and a high density of corner or edge surface sites. in this study, mgo nanoparticle was synthesized using mg(ch3coo)2 and hexamethylenetetramine as starting materials. the structure and optical properties of these particles are investigated by using x-ray diffraction (xrd), scanning electron micros...

the magnetite (fe3o4) – agar nanocomposite was prepared by co-precipitation of fe (iii) and fe (ii) ions for the first time. the obtained samples were characterized by x-ray diffraction, fourier-transform infrared spectroscopy, scanning electron microscopy and transmission electron microscopy. ft-ir results confirm the formation of fe3o4 nanoparticles in agar matrix. the xrd results revealed th...

X-ray micro-diffraction profiles using a synchrotron light source were analyzed via Fourier transformation for single crystal Aluminum and Copper samples subjected to micro-scale laser shock peening. Specifically, the asymmetric and broadened diffraction profiles registered across the shock peen region were observed and analyzed by classic Warren and Averbach (W–A) method [Warren, B.E., Averbac...

The full strain and stress tensor determination in a triaxially stressed single crystal using X-ray diffraction requires a series of lattice spacing measurements at different crystal orientations. This can be achieved using a tunable X-ray source. This article reports on a novel experimental procedure for single-shot full strain tensor determination using polychromatic synchrotron radiation wit...

Research activity: Materials science of magnetic and ferroelectric oxides, semiconductor nanostructures, optoelectronic device design, and characterization of monolithically-integrated GaNand InP-based optoelectronic devices. Primary research interest is in the field of far-IR Ellipsometry, Transmission, and Raman Spectroscopy, Nanoscale High-Angular Resolution X-ray Diffraction, X-ray Standing...

Microcrystals present a significant impediment to the determination of macromolecular structures by X-ray diffraction methods. Although microfocus synchrotron beamlines and X-ray free-electron lasers (XFELs) can enable the collection of interpretable diffraction data from microcrystals, there is a need for efficient methods of harvesting small volumes (<2 µl) of microcrystals grown under common...

Real time, in situ, multiframe, diffraction, and imaging measurements on bulk samples under high and ultrahigh strain-rate loading are highly desirable for micro- and mesoscale sciences. We present an experimental demonstration of multiframe transient x-ray diffraction (TXD) along with simultaneous imaging under high strain-rate loading at the Advanced Photon Source beamline 32ID. The feasibili...