The first total synthesis of Aeruginazole A, prepared via a convergent strategy that involved both solid-phase peptide synthesis and solution phase chemistry and that enabled conservation of the stereochemistry of the intermediates, is reported.

nano-sized titanium dioxide tio2 powder was successfully prepared from its precursor titanium (iv) chloride by a simple and new wet chemical method. ticl4 were used as precursor in hydrogen peroxide, h2o2 and ethanol. this solution was then peptized using nitric acid and heated under reflux at 80°c. their physico-chemical properties were then characterized by transmission electron microscopy (t...

In this research, the Planetary mill was used for mechanical alloying (MA) of Ti and Alpowder mixture with equal at% (Ti50Al50). The effect of various factors, such as process control agent(PCA), speed of rotation of vial and ball-to-powder weight ratio, on process were studied and the bestcondition to synthesis the alloy was determined. Study on X-ray diffraction (XRD) patterns showedthat at p...

Single-crystalline Cd3P2 nanowires (NWs) have been synthesized via a solution-liquid-solid (SLS) mechanism. The lengths of the resulting nanowires can be effectively tuned in the range of 180 nm and 5 μm, and the photodetectors made of the Cd3P2 nanowires exhibited a pronounced photoresponse with high stability and reproducibility.

The synthesis of one-dimensional tubular polymers via a preorganization-polymerization approach is presented. Prior to polymerization, photo-reactive monomers self-assemble into one-dimensional tubular structures in aqueous medium. The supramolecular polymers are subsequently converted into covalent polymers by light-induced anthracene dimerization.

A solution-phase route for the preparation of single-crystalline iron phosphide nanorods and nanowires is reported. We have shown that the mixture of trioctylphosphine oxide (TOPO) and trioctylphosphine (TOP), which are commonly used as the solvents for semiconductor nanocrystal synthesis, is not entirely inert. In the current process, TOP, serving as phosphor source, reacts with Fe precursors ...