A novel solid phase extractor for preconcentration of cadmium at ng L−1 levels has been developed. Cadmium ions were retained on a column packed with sulfur powder modified with 2-mercaptobenzothiazole (2-MBT) in the medium of 1-butyl-3-methylimidazolium hexafluorophosphate ([bmim]+PF6−) ionic liquid. The presence of ionic liquid during modification of sulfur enhanced the retention of cadmium i...

background: the objective of this work was developing a simple and stable time-based on-line setup for assessing the potential of mercury (hg) vapor adsorption of the commercial sorbents used in air sampling and control operation followed by cold vapor atomic absorption spectrometry (cvaas). methods: a special designed separation chamber was used where reduction of the injected hg (ii) solution...

Aminosilanes are routinely employed for charge reversal or to create coupling layers on oxide surfaces. We present a chemical vapor deposition method to pattern mica surfaces with regions of high-quality aminosilane (3-aminopropyltriethoxysilane, APTES) monolayers. The approach relies on the vapor deposition of an aminosilane through a patterned array of through-holes in a PDMS (poly(dimethylsi...

A complete chemical characterization of Moringa oleifera leaves was carried out showing a high content extractives. Extraction kinetics bioactive compounds present in this fraction were performed by conventional and ultrasound assisted extraction (UAE). 50% (v/v) hydroalcoholic mixture led to the highest total phenolic yield solvent extraction, 29.5 ± 0.3 mg per gram moringa leaves. UAE did not...

This paper describes the development of the depth profiling method of ultra trace metal impurities in polytetrafluoroethylene (PTFE) wares based on contamination-free sampling followed by acid-vapor extraction and its application to evaluate the washing method for PTFE wares. A contamination-free sampling process was achieved by scraping the surface of PTFE wares with the cleft face of a silico...

BACKGROUND Based on the noticeable toxicity and numerous application of mercury in industries, removal of mercury vapor through sorbent is an important environmental challenge. PURPOSE OF THE STUDY Due to their highly porous and hollow structure, large specific surface area, light mass density and strong interaction, Single-Walled Carbon Nanotubes (SWCNTs) sorbent were selected for this inves...