X-ray diffraction (XRD) studies are very usefu l for distinguishing crystalline and non-crystalline states. Highl y crystal line substances give patterns with sharp diffraction peaks or spots, whereas liquids or amorphous material s lie between these two extremes, because their chain length is large and it is difficult to attain three-dimensional regularity. However, XRD stud ies of polymers yi...

biosynthesis of silver nanoparticles with small size and biostability is very important and used in various biomedical applications. in the present work, we describe the synthesis of silver nanoparticles (ag-nps) using seed aqueous extract of olea europaea (oe) and its antibacterial activity. uv–visible spectroscopy, x-ray diffraction (xrd), transmission electron microscopy (tem), scanning elec...

in comparison to the previous researches, zro2 nanoparticles with higher surface area (85 m2/g) have been synthesized in this research. the as-prepared zro2 nanoparticles by co-precipitation method were characterized with x-ray diffraction (xrd), scanning electron microscopy (sem) and transmission electron microscopy (tem). the surface area of the sample was characterized by bet method. the eff...

the knoevenagel condensation of aromatic aldehydes with barbituric acid, dimedone and malononitrile occurred in the presence of bf3/nano-γ-al2o3 at room temperature in ethanol. this catalyst is characterized by powder x-ray diffraction (xrd), fourier transform infrared spectroscopy (ft-ir), thermal gravimetric analysis (tga), field emission scanning electron microscopy (fesem) and energy-disper...

The thermal decomposition of hydrotalcites (HTs) with different interlayer anions in the 298-523 K region has been investigated by using transmission electron microscopy (TEM), thermogravimetric analysis (TGA), X-ray diffraction (XRD), and IR, 27Al MAS-NMR and X-ray absorption near-edge structure (XANES) spectroscopy. The thermal stability of the HT with interlayer oxalate was remarkably higher...

A new semiorganic nonlinear optical single crystal of Imidazole Potassium Chloride (IPC) has been grown successfully by slow evaporation method. Colourless, transparent IPC crystal of dimension 5 x 5 x 2 mm has been grown within a period of 21 days. The grown crystal was subjected to single crystal X-ray diffraction (XRD) analysis to determine the lattice parameters. The powder X-ray diffractio...

among different spd techniques, equal channel angular pressing has attracted the most attentions,because of applying large strain to solid bulk materials. in this research, ecap process up to 6passes was carried out on a pure copper and a 6012 al-mg-si alloy with bc route in ecap dieswith φ=120 and ψ=20 and diameter of 20and 10 millimeter respectively. moreover, x-raydiffraction (xrd) system wa...

In this research zinc oxide (ZnO) nano-crystalline powders were prepared by sol-gel method using zinc acetate. The ZnO nanoparticles were characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM), ultraviolet-visible (UV-Vis), Fourier transform infra-red (FT-IR) and energy dispersive X-ray (EDX) spectroscopy. The structure of nanoparticles was studied using XRD pattern. The c...

parkia biglobosa starch was subjected to different heat-moisture treatment (hmt) at different moisture contents (15, 20, 25, and 30%) at 110oc for 16 hours. the content of resistant starch (rs) was the lowest (33.38%) in the untreated native parkia and increased in the samples with hmt-15 (37.79%), hmt-30 (39.64%), hmt-25 (46.63%), and hmt-20 (50.14%), showing significant increase (p < 0.05) in...