نتایج جستجو برای: x ray diffraction zinc oxide electron microscopy

تعداد نتایج: 1233483  

2009
Viorica MUŞAT Monica MAZILU

This paper presents the microstructure, optical and electrical properties of zinc oxide nanorodlike structures deposed on glass substrate by dip-coating method. The crystalline phases and morphology of 1-D nanostructured materials have been investigated using X-ray diffraction and scanning electron microscopy (SEM) techniques. The UV-VIS-NIR spectra and the electrical properties were also measu...

2009
K. Kovnir J. Osswald M. Armbrüster G. Weinberg A. Knop-Gericke Y. Grin

A series of ZnO/Al2O3 mixed oxide samples with varying Zn/Al ratio is prepared by coprecipitation, ageing, drying, and calcination. Samples are investigated in the state after drying and calcination. The applied methods include X-ray diffraction, solid-state 27Al magic-angle spinning nuclear magnetic resonance spectroscopy, transmission electron microscopy and thermogravimetric experiments coup...

Journal: :journal of sciences, islamic republic of iran 2014
m. yarestani a.d. khalaji a. rohani d. das

cobalt oxide (co3o4) nanoparticleshave been synthesized by hydrothermal method using mixture of cobalt(ii)chloride, triton x-100 and koh in an autoclave at 180 °c for 6 h followed by heating at 400 ºc for 3 h in air. the product have been characterized by fourier transform infrared (ft-ir), uv-vis spectroscopy, powder x-ray diffraction (xrd), scanning electron microscopy (sem) and transmission ...

Journal: :applied biotechnology reports 0
seyed javad davarpanah applied biotechnology research center, baqiyatallah university of medical sciences, tehran, iran ramin karimian vahabodin goodarzi farideh piri

copper sulfate was used as a precursor to prepare cuo nanoparticles in reverse micelles (o/w microemulsion).  this is a technique which allows the preparation of ultrafine metal oxide nanoparticles within the size ranging from 50 to 60 nm. the preparation of nano copper (ii) oxide studied was investigated in the inverse microemulsion system. therefore the nucleation of metal particles proceeds ...

پایان نامه :وزارت علوم، تحقیقات و فناوری - دانشگاه صنعتی اصفهان - دانشکده شیمی 1389

in this thesis, a new optically active poly(amide-imide) (pai) was synthesized by the indirect polycondensation reaction of the l-phenylalanine based diacid chloride and 4,4?-diaminodiphenylether in the presence of triethylamine in n-methyl-2-pyrrolidone. the formation of pai was confirmed by ftir, 1h nmr and elemental analysis. in next step, the surface of titanium dioxide (tio2) nanoparticles...

Journal: :iranian chemical communication 2015
maryam movahedi akram hosseinian nasrin nazempour mohadeseh rahimi hossein salavati

in the present work, zno/bi2o3, sno2/bi2o3/bi2o4 mixed oxide, bi2o3 rod-like and sno2 nanoparticle have been synthesized. the obtained samples were characterized by field emission scanning electron microscopy (fe-sem) and x-ray diffraction (xrd). the optical properties of samples were evaluated by uv-vis spectrophotometer. the photocatalytic activity of samples was evaluated by decolorization o...

Journal: :iranian journal of chemistry and chemical engineering (ijcce) 2011
hamid reza ghaffarian, mahboobeh saiedi mohammad ali sayyadnejad ali morad rashidi

zinc oxide (zno) nanoparticles were synthesized by spray pyrolysis method using an aqueous solution of zinc acetate at various concentrations from 5 to 25 wt%. the decomposition of precursor solutions was carried out at 800, 1000 and 1200ºc under different atomizing pressures. the crystal structure and morphology of synthesized nanoparticles were characterized by x-ray diffraction (xrd) spectro...

2015
Nehal A. Salahuddin Maged El-Kemary Ebtisam M. Ibrahim

zinc oxide nanotubes were prepared by a hydrothermal method using zinc nitrate as a precursor. The synthesized nanotubes were characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM), Transmission electron microscopy (TEM), Fourier transform infrared spectroscopy (FT-IR) and their optical properties were characterized using UV -visible spectroscopy. The XRD analysis confirme...

Journal: :international journal of nanoscience and nanotechnology 2015
s. l. sharifi m. h. hosseini a. mirzaei a. salmani oskuloo

the special application of iron-manganese oxide nanocatalysts has been investigated in decomposition of hydrogen peroxide. in this research, iron-manganese oxide nanocomposites were synthesized by co-precipitation, sol-gel and mechanochemical methods using iron (iii) nitrate, iron (ii) sulfate and manganese (ii) nitrate as starting materials. these nanocomposites were prepared on the various ca...

This contribution reports an ecological benevolent route for the fabrication of copper oxide nanoparticles (CuONPs) using Leucaena leucocephala L. leaves extracts at room temperature. Phytochemical screening of the fresh aqueous leaves extract showed the presence of tannins, saponins, coumarins, flavonoids, cardial glycosides, steroids, phenols, carbohydrates and amino acids. Copper oxide parti...

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