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Undoped Zinc oxide (ZnO) nanoparticles as well as ZnO nanoparticles doped with Magnesium (Mg) were synthesized by wet chemical precipitation method using Zinc acetate and Magnesium acetate in Ethylene glycol and distilled water medium. The prepared nanoparticles were characterized with X-ray diffraction (XRD). The XRD patterns show the pattern of typical ZnO nanoparticles and correspond with st...
ZnS nanoparticles of different size have been synthesized using a colloidal particles method. ZnS nanoparticles prepared with capping agent (mercaptoethanol) then were characterized using X-ray diffraction (XRD) and UV-Vis spectroscopy. The particle size of the nanoparticles calculated from the XRD patterns has been found in the range 1.85-2.44nm. Absorption spectra have been obtained using UV-...
The one-step synthesis and characterization of nanostructured metallic platinum microspheres by a low-pressure flat flame technique is presented here. Field emission scanning electron microscopy (FESEM), X-ray diffraction (XRD) and X-ray Photoelectron Spectroscopy (XPS) analyzed the as-derived powders. Collectively, the results obtained from these analyses confirmed the formation of microsphere...
Microwave ferrites require high coercivity for their use as microwave absorbers. Strontium hexaferrite is one of the best material due to its magnetic properties , high coercivity, large unilateral magnetic anisotropy and very low cost in comparison to others make it suitable for the use as microwave components specifically microwave absorber .Strontium nano hexa ferrites were successfully synt...
SrF2:Eu,Ce3+ nanophosphors were successfully synthesized by the hydrothermal method during down-shifting investigations for solar cell applications. The phosphors were characterized by X-ray diffraction (XRD), scanning Auger nanoprobe, time of flight-secondary ion mass spectrometry (TOF-SIMS), X-ray photoelectron spectroscopy (XPS) and photoluminescence (PL) spectroscopy. XRD showed that the cr...
Transparent bubble free phosphate glasses with composition 50P2O5-10Al2O3-20CaO-(20-x)Na2O-xCeO2 (x varying from 0 to 4 mol %) have been prepared using melt quenching technique. The amorphous nature of the prepared glass samples has been confirmed from XRD spectra. The optical absorption coefficient has been determined from the UVvisible absorption spectra. The prepared glass samples have been ...
The thermoluminescence (TL) after excitation by UV or X-rays radiation of alumina-zirconia powders is investigated. The composites present five of the characteristic peaks of zirconia at −170, −145, −90, 0 and 95 °C. After a thermal treatment of mixed oxides, a new peak is observed at −35 °C in TL. This peak reveals the presence of stabilized tetragonal zirconia in the material. Moreover by com...
Chitosan–silver (CS–Ag) nanocomposite materials were synthesized by a simple chemical method. The synthesized CS–Ag nanocomposite contains 20 wt% silver. Silver nanoparticles were synthesized by chemical reduction method as well. The CS–Ag nanocomposite was characterized using Field emission scanning electronic microscope (FESEM), X-ray diffraction (XRD) and Fourier transform infrared spectrosc...
Palladium nanoparticles of average size around 8 nm have been synthesized rapidly by UV irradiation of mixture of palladium chloride and potassium oxalate solutions. A rod-shaped palladium oxalate complex has been observed as an intermediate. In the absence of potassium oxalate, no Pd nanoparticles have been observed. The synthesized Pd nanoparticles have been characterized by powder X-ray diff...
This paper introducesminiPixD: a new, compact system that utilises transmission X-ray imaging and X-ray diffraction (XRD) to locate and identify materials of interest within an otherwise opaque volume. The system and the embodied techniques have utility in security screening, medical diagnostics, non-destructive testing (NDT) and quality assurance (QA). This paper outlines the design of the sys...
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