A simple, rapid and sensitive high-performance liquid chromatographic (HPLC) method for the determination of risperidone in human plasma was developed. An HPLC system based on a Nucleosil C8 column (150?4 mm) and a UV detector (?= 280 nm) were used. A mixture of sodium dihydrogen phosphate buffer-acetonitrile (55:45, v/v) adjusted to pH 6.0 at a flow rate of 1.5 ml min-1 was used as mobile phas...

This paper describes the determination of fatty acid composition of coffee, citrus and rum distillery wastes using reversed-phase high-performance liquid chromatography (RP-HPLC). Lipid extracts of the waste samples are derivatized with phenacyl bromide and their phenacyl esters are separated on a C8 reversed-phase column by using continuous gradient elution with water and acetonitrile. The pre...

This study was aimed at developing RP-HPLC method for determination of natamycin in Turkish yoghurt. Chromatographic separation was achieved on a C8 column (150 mm × 4.6 mm × 5 µm) with a mobile phase of methanol : water : acetic acid (12 : 8 : 1 v/v/v), at 1 mL/min flow rate with a detection of 303 nm. Natamycin was spiked into handmade yoghurt samples and used for validation. The method has b...

a fast, accurate, sensitive, selective and reliable method using reversed-phase high performance liquid chromatography coupled to electrospray ionization ion trap mass spectrometry was developed and validated for the determination of finasteride in human plasma. after protein precipitation with perchloric acid, satisfactory separation was achieved on a zorbax eclipse® c8 analytical column using ...

gamma tocopherol content of 7 iranian sesame seeds (sesamum indicum l.) was determined by high performance liquid chromatography using c8 column and methanol, water and butanol as mobile phase. the gamma-tocopherol content varied from 563 to 1095 mg/kg in oil and 293 to 569 mg/kg in sesame seed and was in broad agreement with the codex range. a large variation was found in the concentration of ...

A directional crystallization of C8-BTBT-C8 in a temperature gradient reduces film roughness and improves in-plane alignment.

a simple, rapid and sensitive high-performance liquid chromatographic (hplc) method for the determination of risperidone in human plasma was developed. an hplc system based on a nucleosil c8 column (150?4 mm) and a uv detector (?= 280 nm) were used. a mixture of sodium dihydrogen phosphate buffer-acetonitrile (55:45, v/v) adjusted to ph 6.0 at a flow rate of 1.5 ml min-1 was used as mobile phas...

a rapid, sensitive and reproducible hplc method using amperometric detector was developed and validated for the analysis of clarithromycin in human plasma. the separation was achieved on a monolithic silica column (mz- c8 125×4.0 mm) using acetonitrile- methanol-potassium dihydrogen phosphate buffer (40:6:54,v/v), with ph of 7.5, as the mobile phase at a flow rate of 1.5 ml/min. the assay enabl...

Gamma tocopherol content of 7 Iranian sesame seeds (sesamum indicum L.) was determined by high performance liquid chromatography using C8 column and methanol, water and butanol as mobile phase. The gamma-tocopherol content varied from 563 to 1095 mg/kg in oil and 293 to 569 mg/kg in sesame seed and was in broad agreement with the Codex range. A large variation was found in the concentration of ...

A simple, rapid and sensitive high-performance liquid chromatographic (HPLC) method for the determination of risperidone in human plasma was developed. An HPLC system based on a Nucleosil C8 column (150?4 mm) and a UV detector (?= 280 nm) were used. A mixture of sodium dihydrogen phosphate buffer-acetonitrile (55:45, v/v) adjusted to pH 6.0 at a flow rate of 1.5 ml min-1 was used as mobile phas...