tio2/zro2 nanocomposite was obtained by the sonochemical technique. in this method, two separate gels containing zirconium and titanium were prepared and mixed together. the precursor sol of zirconium was prepared from an aqueous solution of zrcl4. the precursor titanium tetra isopropoxide (ttip) dissolved in isopropanol. mixing of titanium and zirconium gels was resulted in a yellow tio2/zro2 ...

the effect of temperature variation on the growth of carbon nanotubes (cnts) using thermal chemical vapor deposition (tcvd) is presented. nickel and cobalt (ni-co) thin films on silicon (si) substrates were used as catalysts in tcvd technique. acetylene gas was used in cnts growth process at the controlled temperature ranges from 850-1000 ̊ c. catalysts and cnts characterization was carried out ...

the stabilized zirconia with different cu contents synthesized via sol-gel method. the samples were prepared by hydrolysis and condensation of orgnomatelic sol. after that the result gels were dried at 80 °c and then calcined at various temperatures.  ِ the differential thermal analysis (dta), x-ray diffraction (xrd), field emission scanning electronic microscopy (fesem) and transmission electro...

Nanoporous silicon powder was produced via efficient magnesiothermic reduction. In this work, the thermal effect and reduction process time were investigated on the porous silicon structure. The nanoporous silicon powders were characterized by  X-ray diffraction analysis and field emission scanning electron microscopy. The results demonstrate that porous structure was changed to homogeneous and...

tellurium nanostructures have been prepared by physical vapor deposition method in a tube furnace. the experiments were carried out under argon gas flow at a pressure of 1 mbar. tellurium powder was evaporated by heating at 350°c and 430°c and was condensed on substrates at 110–250°c, in the downstream of argon gas flow. the products were characterized by field emission scanning electron micros...

the study of nucleation mechanism of new grains during severe plastic deformation of magnesium alloys is of great importance to control the characteristics of final microstructures.  to investigate the role of discontinuous recrystallization, a wrought az31 magnesium alloy was deformed by accumulative back extrusion process at 330 °c.  the obtained microstructures were studied using optical and...

in the present investigation surface modification of silica nanoparticles by alumina was carried out by sol-gel process. fourier transform infrared (ftir) and x-ray fluorescence (xrf) confirmed the synthesis of silica and the surface modification as alumina is anchored to silica surface. field emission scanning electron microscopy (fesem) and transmission electron microscopy (tem) investigation...

in this study, tio2 and zno nanofilms were prepared by sol-gel spin-coating method. nanofilms were characterized by x-ray diffraction (xrd), energy dispersive analysis of      x-ray (edx), scanning electron microscopy (sem) and field emission scanning electron microscopy (fe-esm). structural and morphological properties of nanofilms were investigated. the average crystalline size of tio2 and zn...

sio2-coated cobalt ferrite (cofe2o4) nanoparticles were obtained by the hydrolysis of tetraethylorthosilicate in the presence of cofe2o4 nanoparticles in co-precipitation. the effects of sio2coating on the magnetic properties of cofe2o4 nanoparticles were investigated. the structural, morphological and magnetic properties of as-prepared sample were characterization by x-ray diffraction (xrd), f...