Molecular sieves and zeolites are materials whose crystalline frameworks form nanometer or subnanometer pores. A variety of different crystal structures are known having a range of pore sizes. Because the pore sizes are usually smaller than 2 nm, they are classified as microporous materials. Synthesis of microporous materials is usually conducted by the high temperature treatment (80-200 °C) of...

Molecular sieves and zeolites are materials whose crystalline frameworks form nanometer or subnanometer pores. A variety of different crystal structures are known having a range of pore sizes. Because the pore sizes are usually smaller than 2 nm, they are classified as microporous materials. Synthesis of microporous materials is usually conducted by the high temperature treatment (80-200 °C) of...

in this research, a single-stage low-temperature hydrothermal synthesis route was successfully developed for preparation of iron disulfide. the prepared powder was characterized by x-ray diffraction (xrd) and scanning electron microscopy (sem). these analyses showed that nanoparticles were well crystallized, pyrite was the main product and the shape of crystals was nanorod. also, the influences...

In this paper, an in-situ microfluidic control unit (MCU) was designed and applied in a hydrothermal synthesis process, which provides an easy way to localize liquid-phase reaction and realize selective synthesis and direct growth of nanostructures as well as their morphology, all in a low-temperature and atmospheric environment. The morphology was controlled through controlling the amount of a...

Applications of zeolite membranes in separation, chemical sensors, and catalytic membrane reactors have led to extensive studies on their fabrication. To date, mainly silicatebased zeolite membranes of the structure types MFI, DDR, LTA, and FAU have been synthesized on different substrates and evaluated for singleor multiple-gas permeation. Routes for the synthesis of zeolite membranes can be b...

nano-sized γ-al2o3 was synthesized successfully by a simple method using al2(so4)3·18h2o as aluminium source and in the presence of polyethylene glycol (peg 2000). ftir spectroscopy, x-ray diffraction (xrd), scanning electron microscope (sem) and transmission electron microscope (tem) were used to characterize the structure and morphology of synthesized powder. the results showed that peg playe...

microporous hydroxy-sodalite zeolite membranes with different morphologies were synthesized via secondary growth technique with vacuum seeding on tubular α-al2o3 supports at two different synthesis conditions (i.e. two different routes). microstructures of the synthesized membranes were characterized by x-ray diffraction (xrd), scanning electron microscope (sem) and single gas permeation using ...