This paper reports on the precipitation behaviour and microstructural evolution in ~20% cold rolled NbMoV and V single microalloyed low carbon steels during intercritical annealing. The microstructure and precipitation behaviour were studied by optical and scanning/transmission electron microscopy and microanalysis, X-ray diffraction technique and Vickers hardness testing. After intercritical a...

  Abstract   Recovery and recrystallization phenomena and effects of microalloying elements on these phenomena are of great importance in designing thermomechanical processes of microalloyed steels. Thus, understanding and modeling of microstructure evolution during hot deformation leads to optimize the processing conditions and to improve the product properties.   In this study, finite element...

Friction stir processing (FSP) has been considered as a novel technique to refine the grain size and homogenize the microstructure of metallic materials. In this study, two-pass FSP was conducted under water to enhance the cooling rate during processing, and an AZ61 magnesium alloy with fine-grained and homogeneous microstructure was prepared through this method. Compared to the as-cast materia...

Continuous solidification experiments were carried out with Cu-Bi-Sn alloys under the effects of Electric Current Pulses (ECPs). A model describing the microstructure evolution was developed. The formation of the microstructure in the continuously solidified alloys was calculated. The calculations demonstrated that ECPs mainly affect the solidification process through changing the energy barrie...

It is a well known fact that at high sampling frequencies, the contamination of microstructure noise causes the Realized Variance to be a biased measure of the Integrated Variance. Recent developments in this field propose sampling on lower frequencies, sub-sampling techniques, or bias corrections using the autocorrelation patterns in the data. In this paper we propose a structural decompositio...

7000 series aluminum alloys are widely used in the automotive industries for structural lightweight components due to their exceptional high strength to weight ratio. however, this class of aluminum alloy is difficult to join by conventional fusion welding techniques so friction stir welding (fsw) widely is used for welding this alloys. the process has been demonstrated to be effective and is c...

Near-net shape processes, such as laser metal deposition (LMD), offer a unique combination of process flexibility, time savings, and reduced cost in producing titanium alloy components. The current challenge in processing titanium alloys using LMD methods is understanding the complex microstructural evolution as a part is fabricated layer by layer. The microstructure is affected by the repeated...

Four dimensional (4D, or 3D plus time) X-ray tomographic imaging of phase changes in materials is quickly becoming an accepted tool for quantifying the development of microstructures to both inform and validate models. However, most of the systems studied have been relatively simple binary compositions with only two phases. In this study we present a quantitative dataset of the phase evolution ...

A method to determine material parameters by comparing the evolution of experimentally determined 3D microstructures to simulated 3D microstructures is proposed. The temporal evolution of a dendritic solid-liquid mixture is acquired in situ using x-ray tomography. Using a time step from these data as an initial condition in a phase-field simulation, the computed structure is compared to that me...

In order to study the influence on the mechanical properties caused by microstructure evolution of metal powder in extreme environment, 3D real-time observation of the microstructure evolution of Al-Ti mixed powder in high temperature and microwave compound fields was realized by using synchrotron radiation computerized topography (SR-CT) technique; the spatial resolution was enhanced to 0.37  ...