نتایج جستجو برای: microwave assisted solution combustion synthesis

تعداد نتایج: 1047358  

Journal: :international journal of bio-inorganic hybrid nanomaterials 0

glycerol mono-oleate (gmo) was produced by direct esterification reaction with amberlyst 16 resin catalysts with the efficiency of 86% and was used as a surfactant for synthesis of cofe2o4 nano-particles by surfactant-assisted microwave method. fourier transform infrared spectroscopy (ft-ir), x-ray diffraction (xrd) and scanning electron microscopy (sem) were used to consider the structural and...

2015
Jonathan Wooten VALENTINE WOOTEN Peng George Wang Jonathan Valentine Wooten Maged Henary Gangli Wang Yunpeng Liu Kristina Gardner Zaikuan Yu

Glycoscience is an emerging field of science that focuses on the study of the structure, biosynthesis, biology, and evolution of saccharides (sugars). It covers a broad range of subjects including microwave-assisted synthesis as well as sphingolipid synthesis. In this field, knowledge is limited due to the complexity of carbohydrates and their derivatives. Therefore, it is all the more importan...

Journal: :Journal of combinatorial chemistry 2010
Ya-Shan Hsiao Gorakh S Yellol Li-Hsun Chen Chung-Ming Sun

A new multidisciplinary synthetic approach comprising polymer-support synthesis, microwave-assisted synthesis, and multicomponent condensation facilitates synthesis of triaza-fluorenes library with a set of advantages such as rapid process, simple purification, and structural diversity in one shot. Microwave-assisted multistep synthetic protocol was used to construct the benzimidazole ring on s...

2011
Idalia Bilecka Martin Kubli Esther Amstad Markus Niederberger

Combination of the surfactant-free nonaqueous sol–gel approach with the microwave technique makes it possible to synthesize Fe3O4, CoFe2O4, MnFe2O4, and NiFe2O4 nanoparticles of about 5–6 nm and with high crystallinity and good morphological uniformity. The synthesis involves the reaction of metal acetates or acetylacetonates as precursors with benzyl alcohol at 170 C under microwave irradiatio...

This paper reports the synthesis and characterization of photocatalyst CdS nanoparticles for investigation of photocatalytic degradation of 2,4,6-trichlorophenol. CdS nanoparticles were synthesized by the microwave-assisted sol-gel method and characterized by various techniques such as X-ray diffraction, filed emission scanning electron microscopy, energy dispersive spectroscopy, Fourier transf...

Journal: :The Journal of organic chemistry 2005
Ji-Feng Liu Mira Kaselj Yuko Isome Jennifer Chapnick Bailin Zhang Grace Bi Daniel Yohannes Libing Yu Carmen M Baldino

[reactions: see text] One-pot total syntheses of the quinazolinobenzodiazepine alkaloids sclerotigenin (1), (+/-)-circumdatin F (2), and (+/-)-asperlicin C (3) via novel microwave-assisted domino reactions were achieved in 55%, 32%, and 20% yields, respectively, from commercially available starting materials. A two-step total synthesis of (+/-)-benzomalvin A (4) was accomplished with an overall...

This paper reports the synthesis and characterization of photocatalyst CdS nanoparticles for investigation of photocatalytic degradation of 2,4,6-trichlorophenol. CdS nanoparticles were synthesized by the microwave-assisted sol-gel method and characterized by various techniques such as X-ray diffraction, filed emission scanning electron microscopy, energy dispersive spectroscopy, Fourier transf...

2014
J. J. Shah Krishnapriya Mohanraj

A green chemistry approach for organic synthesis is described here, which involves microwave exposure of reactants in presence or absence of solvents. A novel and simple method has been developed for the synthesis of some benzotriazole derivatives under microwave irradiation. In addition, these compounds were synthesised also by conventional heating procedures for comparison. All the compounds ...

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