Differences between solution and solid state 13C nuclear magnetic resonance spectra of some amphetamines namely, 3,4-methylenedioxyamphetamine HCI, (R.S)-MDA HCI, the methyl derivative 3,4-methylenedioxy-N-methylamphetamine x HCI, (R,S)-MDMA x HCI, the ethyl derivative, (R,S)-MDEA x HCI, and the analogues (R,S)-methamphetamine HCI, (-)-ephedrine x HCI (the 3R,2S enantiomer as numbered here), an...

Capillary zone electrophoresis was applied for the determination of amphetamine and related substances in seized drugs. A buffer made of 0.1 M phosphoric acid adjusted to pH 3.0 with triethanolamine was selected. With this background electrolyte, triethanolamine is adsorbed to the capillary wall and the electroosmotic flow is reversed. This gives rise to peaks with good symmetry, high efficienc...

The title compound, 2C(21)H(34)N(4)O(3)S(2+)·4I(-)·5H(2)O, was prepared exclusively as the E isomer by methyl-ation of the corresponding N-phenyl-pyridin-4-amine. There are two symmetry-independent mol-ecules in the asymmetric unit with no significant differences in bond lengths and angles. The aromatic rings are not coplanar with the pyridin-4-imine groups, as indicated by the C-N-C-C torsion ...