stoichiometric tetragonal bal-xsrxtio3 (x = 0.23) nanopowders were prepared by stearic acid gel(sag) method using barium stearate, strontium stearate, tetrabutyl titanate as ba, sr, ti sourcesand stearic acid as complexing reagent. thermal analysis including differential thermogravimetric(dtg) and tg, fourier transform infrared spectrometry (ftir), x-ray diffraction (xrd) andtransmission electr...

zinc oxide (zno) nanopowders were synthesized by the sol–gel method from an ethanol solution of zinc sulfate heptahydrate in the presence of diethylene glycol surfactant. detailed structural and microstructural investigations were carried out using x-ray diffraction (xrd), high-resolution transmission electron microscopy (hrtem), field emission scanning electron microscopy (fe-sem), fourier tra...

pure barium zirconate nanopowders were successfully prepared in wet-chemistry synthesismethod, using barium stearate and tetra-n-butyl zirconate as ba, zr sources and stearic acid ascomplexing reagent. the gel was calcined at 800 and 900 °c in air. results of thermal analysisare given, including both dtg and tg. fourier transform infrared spectrometry (ftir), x-raydiffraction (xrd), transmissio...

................................................................................... viii CHAPTER 1. INTRODUCYION ........................................................... 1 1.1 Motivation ................................................................................. 1 1.2 Outline ..................................................................................... 2 CHAPTER 2. SOL-GEL PHOT...

to improve the corrosion protection of copper metal, 0.01m concentration of 1h-1,2,4-triazole-3-thiol (tat) was incorporated into the hybrid sol-gel monolayers containing 3-glycidoxypropyltrimethoxysilane (gptms) and tetraethoxysilane (teos). it was further subjected to hydrolysis and condensation reaction to form a sol-gel matrix. the tat-doped hybrid sol-gel coating was applied over the coppe...

Light transducing phycobiliproteins are encapsulated in optically transparent sol-gel matrices. Absorption and fluorescence spectroscopies are used to characterize the effect of the sol-gel encapsulation on the conformation and aggregation states of the three major phycobiliproteins present in phycobilisomes: phycoerythrin, phycocyanin, and allophycocyanin. It is found that the effects of sol-g...