نتایج جستجو برای: non isothermal heating rates
تعداد نتایج: 1751253 فیلتر نتایج به سال:
In this research, the thermal stability and decomposition kinetics of pentaerythritol tetranitrate (PETN) and Pentastite explosives have been studied experimentally using non-isothermal differential thermal analysis (DTA) and thermo-gravimetric (TG) methods at heating rates of 4.0, 6.0, 8.0 and 10.0 °C/min. The kinetic parameter of activation energy (Ea) and critical ignition temperature fo...
Isothermal nucleic acid amplification tests (NAAT) in a Lab-on-a-Chip (LoC) format promise to bring high-accuracy, non-instrumented rapid tests to the point of care. Reliable rapid tests for infectious diseases allow for early diagnosis and treatment, which in turn enables better containment of potential outbreaks and fewer complications. A critical component to LoC NAATs is the heating element...
Artificial diagenesis of the intra-crystalline proteins isolated from Patella vulgata was induced by isothermal heating at 140 °C, 110 °C and 80 °C. Protein breakdown was quantified for multiple amino acids, measuring the extent of peptide bond hydrolysis, amino acid racemisation and decomposition. The patterns of diagenesis are complex; therefore the kinetic parameters of the main reactions we...
The scale up of an isothermal micro-trickle bed reactor operated under radio frequency (RF) heating has been performed. The effect of the reactor length, tube diameter and number of parallel tubes on the temperature non-uniformity parameter has been studied. The axial and radial temperature profiles were calculated using a 2D convection and conduction heat transfer problem with heat transfer pr...
The influence of calcination time on the phase transformation and crystallization kinetics of anodized titania nanotube arrays was studied using in-situ isothermal and non-isothermal synchrotron radiation diffraction from room temperature to 900 °C. Anatase first crystallized at 400 °C, while rutile crystallized at 550 °C. Isothermal heating of the anodized titania nanotubes by an increase in t...
The thermo-hydraulic-mechanical behaviour of a large in situ heating test, the Buffer/Container Experiment (BCE), carried out at Atomic Energy of Canada’s underground research laboratory, is considered. The work can be seen as an extension of the authors’ previous research, investigating the behaviour of a large-scale test, the socalled ‘isothermal test’, to now include heating effects. Suggest...
poly(ethylene adipte) and poly(ethylene adipate)/silica nanocomposite (pead/sio2) containing 3 wt. % sio2 were prepared by an in situ method. the examinations on the non-isothermal crystallization kinetic behavior have been conducted by means of differential scanning calorimeter (dsc). the avrami, ozawa, and combined avrami and ozawa equations were applied to describe the crystallization kinet...
Carbon monoxide (CO) and carbon dioxide (CO2) emissions during a spontaneous heating event in a coal mine are important gases to monitor for detecting the spontaneous heating at an early stage. However, in underground coal mines, the CO and CO2 concentrations and their related fire ratios may be affected by mine ventilation. In this study, CO and CO2 emissions from spontaneous heating of a U.S....
One of the characteristics of solid organic compounds and especially organic explosives is thermal behavior and kinetic of thermal decomposition. The activation energy, Arrhenius constant and model of solid state reaction as kinetic triplet can be obtained by study thermal decomposition kinetic in a solid state reaction. In the present work, the non-isothermal differential thermal analysis (DTA...
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