نتایج جستجو برای: sol gel process

تعداد نتایج: 1408468  

پایان نامه :دانشگاه تربیت معلم - تهران - دانشکده علوم پایه 1389

در این پایان نامه ابتدا نانو ذرات دی اکسید تیتانیم یا تیتانیا به روش شیمیایی sol-gel در دو فاز آناتاز و روتایل سنتز شده است. سپس این نانو ذرات به کمک الگوهای پراش اشعه x (xrd) طیف سنجی uv-vis و میکروسکوب الکترونی رویشی (sem) مشخصه یابی شده است. الگوی پراش اشعه x و تصاویر sem تشکیل ساختارهای نانومتری دی اکسکیدتیتانیم تهیه شده و به روش sol-gel را تایید می کنند ساختار و میانگین اندازه نانو ذرات به...

Journal: :Journal of Materials Research 2022

Abstract Sol–gel derived hydroxyapatite coatings on metallic implants are important to promote their osseointegration and biocompatibility. However, such generally suffer from drawbacks that limit implant longevity. In this study, the sol gel process prepare was optimized used deposit a layer Ti6Al4V. Samples were pretreated by thermal oxidation, sol–gel coating, anodization produce titanium di...

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In this study, zirconium carbide nanoparticles were synthesized by the sol-gel method in the alcoholic system. The sol was prepared in a three-component alkoxide-water-alcohol system based on the chemical sol-gel process under acidic conditions and at pH = 5. Zirconium n-propoxide, furfuryl alcohol were used as raw materials. After the hydrolysis process and formation of the gel, the initial po...

Bahram Mellatnavaz Hadi Adelkhani, Hossein Roohi Mansoor Noorbakhsh

As we know sol-gel is one of the most important techniques for thin film preparation. In this paper, high transmission silica thin films have been prepared by dip-coating process from a new silicon-alkoxide solution. The prepared sol was stable for 45 days which is very important to characterize the coating process. The optical properties as a function of aging time, withdrawal rate, and he...

Journal: :Langmuir : the ACS journal of surfaces and colloids 2009
Ruben Mercadé-Prieto Sundaram Gunasekaran

The cold gelation of preheated whey protein isolate (WPI) solutions at alkaline conditions (pH>10) has been studied to better understand the effect of NaOH in the formation and destruction of whey protein aggregates and gels. Oscillatory rheology has been used to follow the gelation process, resulting in novel and different gelation profiles with the gelation pH. At low alkaline pH, typical sol...

ZnO nanorods were prepared using dimethylamine (DMA) controlled Sol-Gel process. Dimethylamine was added as an additive to control the sol-gel process for growing ZnO nanorods. DMA would exhibit stabilizing effect, promote dissolution of precursor and control the rate of sol-gel reactions because of its basic nature and significant miscibility. The Structural and microstructural properties of t...

Journal: :iranian journal of chemistry and chemical engineering 0

to improve the corrosion protection of copper metal, 0.01m concentration of 1h-1,2,4-triazole-3-thiol (tat) was incorporated into the hybrid sol-gel monolayers containing 3-glycidoxypropyltrimethoxysilane (gptms) and tetraethoxysilane (teos). it was further subjected to hydrolysis and condensation reaction to form a sol-gel matrix. the tat-doped hybrid sol-gel coating was applied over the coppe...

2004
ZHONGPING CHEN

Light transducing phycobiliproteins are encapsulated in optically transparent sol-gel matrices. Absorption and fluorescence spectroscopies are used to characterize the effect of the sol-gel encapsulation on the conformation and aggregation states of the three major phycobiliproteins present in phycobilisomes: phycoerythrin, phycocyanin, and allophycocyanin. It is found that the effects of sol-g...

2000
JOHN F.T. CONROY MARY E. POWER JASON MARTIN BRIAN EARP BOUVARD HOSTICKA CHARLES E. DAITCH PAMELA M. NORRIS

A novel, high hydrolysis ratio sol-gel route for the biocompatible production of macroporous silica gels is presented. This route exploits the two step nature of the gelation reaction to remove undesired alcohol by-products from an acidic aqueous sol prior to gelation. These alcohol-free sols will gel when the pH is raised to the physiologic range in a two-step, acid/base catalyzed process. Fur...

2004
V. K. Parashar

We have applied the sol-gel process to generate optical microstructures in glass using in-house developed sol-gel materials. The synthesis of our sol-gel glass materials is based on the formation of particles of controlled size from organo-metallic compounds. The overall shrinkage during annealing of the gel material is negligible and does not imply crack formation. Silica, titania and binar y ...

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