A sensitive quantification of decabrominated diphenyl ether (deca-BDE) was achieved by optimizing the injection temperature, pressure and column system with gas chromatography mass spectrometry in selected ion monitoring mode. A simple one-step cleanup method with acid silica gel column chromatography showed the optimum efficiency and minimum matrix interference. Ultrasonic-assisted extraction ...

In order to improve the traditional methods of procyanidins extracting, ultrasonic-assisted filtration was used in the process of extracting proan-thocyanidin which was from membrane concentration of grape seed. Through the mechanism analysis of ultrasonic-assisted ultrafiltration, ultrasonic is able to alleviate the phenomenon of concentration polari-zation, so the efficiency of extracting pro...

Background: Illicium verum is widely cultivated in southern China especially in Guangxi province. Its fruits has been traditionally used in Chinese medicine. In recent years, it has been the industrial source of shikimic acid. Usually the residues after extracting shikimic acid are treated as waste. Thus, the aim of this study was to optimize the extraction conditions of cellulase-ultrasonic as...

phenolic compounds, especially those of plant origin, constitute an essential part of the human diet, and are of considerable interest due to their antioxidant properties. in this study, ultrasound-assisted extraction (uae), microwave-assisted extraction (mae), as well as maceration extraction (me) methods were applied for phenolic compounds’ extraction from pistachio green hull. response surfa...

Blueberry leaf as materials, ethanol ultrasonic assisted extraction of blueberry polyphenols, concentration and solid-liquid ratio on time leaves influence the yield polyphenols were researched, orthogonal experiment to optimize technological conditions polyphenol was used. The results showed that optimal from follows, 9.06% with 4min time, 80% 1:45 (g/mL) ratio. Ultrasonic is a convenient high...

Background and objectives: Stevia rebaudiana Bertoni is a herbaceous and a small shrub of the Compositae family. It is native to certain regions of South America. Since 1970s, Stevia extracts have been extensively used in many countries as a sugar substitute. Stevia is cultivated in many countries: Paraguay, USA, Mexico, Central America, Japan, China,...

It is reported that salvianolic acid B, a bioactive phenolic compound contained in the root of Salvia miltiorrhiza, exhibits a much stronger activity in free radical scavenging and antioxidance than those of vitamin E. When a conventional refluxing method is adopted to extract salvianolic acid B from the root, in which the materials are subjected to higher temperature and longer time, the yield...

The influence of oil rate and quality of rice bran oil by enzymatic extraction ultrasonic assisted were studied through designed experiment. The optimum enzymatic hydrolysis conditions were determined by the way of the orthogonal test. The results showed: after lipase enzyme in the rice bran (40 mesh sieve) was killed by the hot steam, the solution compounding material liquid ratio was 1:5 (W/V...

When harvesting corn, corn silk was discarded as waste, including the compounds isolated and identified from such flavonoids, sterols, alkaloids, polysaccharides, organic acids, volatile oils, trace elements, multivitamins. It not only pollutes environment but also wastes resources. In this paper, extraction methods commonly used for extracting flavonoids were reviewed, reagent method, enzymati...

Teh ultrasound-assisted magnetic stirrer was used as an effective extraction technique for teh evaluation of total phenolic contents (TPC) and antioxidant potential of ten Pakistani brown rice cultivars. For this purpose, ultrasonic (240W frequency 50/60 Hertz) assisted magnetic stirrer coupled with three solvents methanol, ethanol, and isopropanol in pure and aqueous fractions (80:20) were...