S-doped and bare mesoporous TiO2 were prepared using titanium tetraisopropoxide and thiocarbamide as raw materials. Prepared materials were characterized by means of fourier transform infrared spectroscopy FT-IR, thermogravimetry-differential scanning calorimetry (TG-DSC), X-ray diffraction (XRD), UV–Vis absorption spectroscopy, Brunauer–Emmett–Teller (BET) specific surface area and Barrett–Joy...

in this study silver/poly vinyl alcohol (pva) and silver/poly vinyl pyrrolidone (pvp) nanocomposites were prepared via reduction of silver salt by employing dmf (n, n`- dimethyl formamide) as a reducing agent. effects of protective agents such as pva and pvp were also described here. we show that the acidic ph of pvp solution also affects the interaction between protective agents and silver nan...

Sol-gel technique was used to coat multiwall carbon nanotubes (MWCNTs) with anatase titania to increasing the surface area and improve the photocatalytic activity of TiO2. Room temperature ballistic conduct of MWCNT combined with semiconducting behavior of anatase brought about a photocatalytic improvement of ~37 % with respect to the highest methyl orange decolorization flair. For characteriza...

In this work, H3PW12O40 (PPT) and nano-sized titania supported on urea formaldehyde (UF) resinwas prepared via an impregnation method. The prepared sample was characterized by X-raydiffraction (XRD), UV-Vis spectrophotometer, Fourier transform infrared spectroscopy (FT-IR),scanning electron microscopy (SEM) and energy-dispersive X-ray spectroscopy (EDX). The photocatalyt...

Chemical grafting of Polyaniline (PAni) and chitosan (CS) as has been carried out with formaldehyde as grafting agent and ammonium persulfate as an initiator. For this reason aniline monomers were copolymerized with chitosan and were chemically polymerized. The synthesized copolymer was Characterized using Fourier transform infrared spectroscopy (FTIR), UV-Visible, scanning electron microscopy ...

To obtain accurate and consistent measurements from circular dichroism (CD) instruments over time and from different laboratories, it is important that they are properly calibrated. The characteristics of the available reference materials are not ideal to ensure proper calibration as they typically only give peaks in one or two spectral regions, and often have issues concerning purity and stabi...

cu2o nanoparticles were synthesized by thermal treatment in liquid paraffin without any inert gas protection using nano structures of schiff base copper (ii) complex (1) as precursor. liquid paraffin was used as solvent and reductant. span 80 was applied to control the morphology of cuprous oxide nanoparticles. the nano structure of the complex was characterized by x-ray diffraction measurement...

Plant-mediated synthesis of metal oxide nanoparticles is a promising alternative to the traditional method of physical and chemical synthesis. In this paper, we report the green synthesis of zinc oxide nanoparticles (ZnONPs) by a biological method. During the study, Zinc oxide nanoparticles were synthesized by Allium sativum skin (garlic skin) extract. Formation of zinc oxide nanoparticles has ...

the interaction between nano-sio2 and lysozyme was investigated by the method of uv-visible  detection and fluorescence spectroscopic techniques. the thermal denaturation of lysozyme has been investigated in the presence and absence of nano-sio2 over the temperature range (293-373) k in different buffers and ph values, using temperature scanning spectroscopy. the presence of nano-sio2 caused th...

We demonstrate reversible photoisomerizaton of azobenzene molecules on a single gold nanoparticle surface with alternating UV and visible irradiation, which is monitored by plasmon resonance Rayleigh scattering spectroscopy and stimulated by the discrete-dipole approximation method.