A simple and sensitive method for routine analysis of TSNAs in mainstream cigarette smoke has been developed. Cigarette smoke particulate matter was collected according to ISO 4387. The particulate matter was extracted with methylene chloride, cleaned up with an Agilent Bond Elut Alumina B SPE cartridge, and analyzed using an Agilent 7000A Triple Quadrupole GC/MS system with an Agilent J&W DB-3...

The aim of this study was to evaluate the bone regeneration of hydroxyapatite (HA)/alumina bilayered scaffold with a 3 mm passage-like medullary canal in a beagle tibia model. A porous HA/alumina scaffold was fabricated using a polymeric template-coating technique. HA/alumina scaffold dimensions were 10 mm in outer diameter, 20 mm in length, and with either a 3 mm passage or no passage. A 20 mm...

Increasing uses of engineered nanoparticles (ENPs) in commercial products and industrial applications has eventually resulted to their releases into atmospheric, terrestrial, and aquatic environments. However, knowledge gaps in ENPs toxicity, fate, and behaviour currently limit our ability to quantify risk assessment of materials with nanoscale dimensions, and therefore, the extent of the resul...

THE following comments are directed to the sections (2) ‘‘revisit to the grain growth problems in alumina’’ and (3) grain growth without a liquid phase in the article of concern. The purpose of this comment is to challenge the authors’ assertions and refute the following arguments, namely, first that ‘‘MgO can be considered a very effective grain growth promoter in the sintering of alumina,’’ s...

Egyptian Petroleum Research Institute, Nasr City, Cairo, Egypt. Chemistry department, Faculty of Science, Taif University, KSA. _________________________________________________________________________________________ Nine alumina samples of various modification techniques were subjected to thermal analysis via thermogravimetric analysis (TGA) and differential thermal analysis (DTA), in order t...

Simultaneous application of colloidal processing and liquidforming additives to alumina resulted in a sintered density of >99% in 1 h at a temperature as low as 1070°C for a commercial high-purity alumina powder at a total dopant level of 2 mol%. The additives were 0.9% CuO + 0.9% TiOz + 0.1% B 2 0 3 + 0.1% MgO. At higher temperatures or after prolonged sintering, the doped alumina ceramic deve...

A comparison has been made of the infrared spectra of alumina with molybdenum oxide alumina in both the oxidized and reduced forms. In the case of molybdena-alumina prepared via adsorption of gaseous MoOp(OH)t, the spectra show that a practically complete monolayer of Mo6+ oxide covers the alumina. After reduction with hydrogen the hydroxyls of the carrier appear. From the reversibility of redu...

Red mud, which could cause numerous problems to the environment, is a hazardous waste generated from alumina smelting industry. In general, storage and harmless utilization of red mud are hard implement due its fine particle size high alkalinity. This study put forward novel process separate iron (MgFe2O4) (Al2O3) in by magnetization sintering method. The magnesium oxide was added transform non...

a column of alumina modified with sodium dodecyl sulfate (sds) and dimethylglyoxime (dmg) was prepared for the preconcentration of trace nickel from water samples for flame atomic absorption spectrometry (faas) determinations. under optimized conditions (ph=7.0; flow rate: 20 mlmin-1) nickel was retained on the column. the nickel collected on the column was eluted with 5 ml of 1 m nitric acid. ...

Porous alumina film on aluminum with gel-like pore wall was prepared by a two-step anodization of aluminum, and the corresponding gel-like porous film was etched in diluted NaOH solution to produce alumina nanowires in the form of densely packed alignment. The resultant alumina nanowires were reacted with NH(3) and evaporated aluminum at an elevated temperature to be converted into densely pack...