The performance of nanocomposite electrodes prepared by controlled ball-milling of TiS₂ and a Li₂S-P₂S₅ solid electrolyte (SE) for all-solid-state lithium batteries is investigated, focusing on the evolution of the microstructure. Compared to the manually mixed electrodes, the ball-milled electrodes exhibit abnormally increased first-charge capacities of 416 mA h g(-1) and 837 mA h g(-1) in the...

PLGA is a biodegradable polymer utilised widely in pharmaceutical research for the encapsulation of a wide range of drugs as nano particulate systems. This study investigates the impact of rotary ball milling on the physical properties of PLGA and its influence on nanoparticle formation prepared using the solvent displacement technique. By applying mechanical stress to the polymer and altering ...

The effect of CaO on the formation of β- and γ-zirconia nanoparticles from α-zirconia was investigated and their stability evaluated via mechanical activation. α-ZrO2+8.5wt%CaO powder was milled for 2-150 hours with ball-to-powder weight ratios (BPWR) of 40:1 and 60:1. Structural evaluations were conducted using X-Ray diffraction and scanning electron microscope (SEM). Thermal analysis wa...

This study showed pronounced changes in the Raman scattering of silicon powder during high-energy ball milling. The powders were milled for 1–18 h in a steel ball mill in argon. The approximate pressure imposed on particles was 2 GPa. The spectra of the as-milled powders were compared with the initial silicon. It was found from the Raman peak position shifts that milling generated strains in th...

The hcp-fcc transformation induced in cobalt powder by ball milling at room temperature was studied using the excess Gibbs free energy for the metals, in nanometric form, to calculate the activation barriers that the atoms must overcome for the phase transformation to occur. The crystalline component of the nanocrystaline cobalt produced in our laboratory, via ball milling, was analized using t...

Forsterite (Mg2SiO4) powder was synthesized using magnesium and talc with assistance of ball milling. Manganese doped forsterite was prepared at weight percentage of 0.05%, 0.1%, 0.2%, 0.5% and 1.0wt% by adding manganese oxide before ball milling. The undoped and manganese doped forsterite were sintered at temperature of 1000°C, 1100°C and 1200°C. The Vickers hardness, fracture toughness and Yo...

The recently developed protocol for isolating enzymatic mild acidolysis lignins (EMAL) coupled with the novel combination of derivatization followed by reductive cleavage (DFRC) and quantitative (31)P NMR spectroscopy were used to better understand the lignin isolation process from wood. The EMAL protocol is shown to offer access at lignin samples that are more representative of the overall lig...

Due to the large thermal neutron absorption cross section of 10B, B4C-Al composites have been used as neutron absorbing materials in nuclear industries, which can offer not only good neutron shielding performance but also excellent mechanical properties. The distribution of B4C particles affects the mechanical performance and efficiency of the thermal neutron absorption of the composite materia...

The NiO and Fe2O3 powders were mixed by the high-energy ball-milling, followed a sintering of mixture at 1340°C for 0.5 h. XRD, SEM, DSC, size measurements preformed to study microstructure evolution in ball-milled sintered ones, as well. It showed that ball-milling processes resulted severe lattice distortion powder Fe2O3, but only slight NiO. Meanwhile, solid solution iron atoms into was also...

Damage to carbon nanotubes (CNTs) during the fabrication process of CNT reinforced composites has great influence on their mechanical properties. In this study, the 2014 Al with powder sizes of 20, 9 and 5 μm was selected to study the effect of initial particle size on the damage to carbon nanotubes (CNTs) during ball milling. The result shows that for CNTs in the ball milled CNT/Al (with powde...