This paper studies the synthesis and the design of methanol recovery system for TAME reactive distillation process using extraction column with water as a solvent. The design of the extraction column system has not been studied in the literature. The effect of operating conditions such as solvent flowrate, extraction column temperature, and number of equilibrium trays are studied. It is found t...

  The simulation of distillation columns is an essential step in design, optimization, and rating. In this paper, a new procedure has been proposed for the initial estimation of column profiles based on modified Kremser’s group method for simple and/or complex columns. The effect of this initialization algorithm on simulation procedure has been studied through two examples. The results show sig...

Startup of distillation columns is one of the most difficult operations of chemical processes. Since it often lasts a period of time, leads to off-products and costs much energy, optimization of startup operating policies for distillation columns is of great interest in process industry. Most previous studies on column startup have been restricted to theoretical investigations such as modeling,...

ABSTRACT-This paper proposed a control scheme based on fuzzy logic for a methanol water system of bubble cap distillation column. Fuzzy rule base and Inference System of fuzzy (FIS) is planned to regulate the reflux ratio (manipulated variable) to obtain the preferred product composition (methanol) for a distillation column. Comparisons are made with conventional controller and the results conf...

A rigorous model for the simulation of the dynamic behaviour of distillation column including pressure relief has been developed. This model allows the analysis of the influence of different disturbances (failures) on the dynamic behaviour of a methanol/water column. Disturbances of the cooling medium supply to the condenser and the reflux stream have been examined. In this paper the results of...

Simultaneous control of overhead and bottoms composition in a binary distillation column using reflux and steam flow as the manipulated variables often proves to he particularly difficult because of the interaction inherent in the process. The development of model based control ( M E ) theory in the past 20-25 years has provided a framework which caters for the above distillation control proble...

Distillation separates compounds by the variation in how effortlessly they vaporize. The two main types of standard distillation comprise unremitting distillation and batch distillation. Unremitting distillation, as the name says, unremittingly takes a feed and separates it into two or more products. Batch distillation takes on lot (or batch) at a time of feed and splits it into products by sel...

Distillation columns with a high-purity product (down to 7 ppm) have been studied. A steady state model is developed using a commercial process simulator. The model is validated against industrial data. Based on the model, three major optimal operational changes are identified. These are, lowering the location of the feed & side draw streams, increasing the pressure at the top of the distillati...