Biginelli-type reaction was developed by means of a three-component condensation of analdehyde, ethyl acetoacetate, urea or thiourea and nano alumina sulfonic acid (Al2O3-SO3H)(NASA) as catalyzed. It is carried out under different conditions. In all conditions, the desiredproducts are obtained in high yields after relatively short reaction times. Nevertheless, thereactions proceeded faster and ...

in this research, b4c-ni cermet coating was sprayed on the surface of 4130 steel from b4c and ni feed-stockpowders using high velocity oxy-fuel (hvof) method. in order to characterize the tribological behavior of thecoating, ball on disk wear tests were done at the ambient temperature and under the loads of 1, 3 and 5 n.phase analysis of the coating after spraying was studied by x-ray diffracto...

The dried nitrate-urea gels exhibit the combination of autoicatatric combustion behavior and ultrasonic, whichcan be used to synthesize the nanocatalyst ferrite powders. Cu and Ni Unites nanocatalyst powders sithcomposition of Caned], and NiFe204 were synthesized by a sol-gel auto catalnic combustion process. Themolar ratio between metal ions and urea was 11.2. The sob gel process was done at 8...

A simple, inexpensive and one-step synthesis route of Ag-TiO2 nanoparticles by arc discharge method isreported. The resulting nanoparticles were characterized using X-ray diffraction and scanning electronmicroscopy. X-ray diffraction patterns demonstrate dominance of rutile to anatase phase in TiO2 andformation of silver metal on TiO2 after arc discharge process. Scanning electron microscopy im...

Supercapacitors are energy storage devices that can cleanly and efficiently meet the growing demand. The presentwork describes synthesis of nanoparticles cobalt ferrite (CoFe2O4) by combustion method their use with activated carbon (AC) to manufacture supercapacitors. In order study influence composition on electrochemical properties, supercapacitors three different compositions were produced: ...

Mast cells were identified by electronmicroscopy in the alveolar wall of the lung in 20 subjects (10 normal, 10 abnormal). A quantitative and qualitative study was made of the mast cells. In the normal lung there was an average concentration of 350 mast cells/mm2 of alveolar wall and in the abnormal 523/mm2. Mast cells occupied approximately 1.6-2.1% of the area of the alveolar wall. There was ...